C₂₈H₃₈N₆O₄S

Base Information

• Chemical Name: C₂₈H₃₈N₆O₄S
• CAS No.: 1446250-90-3
• Molecular Formula: C₂₈H₃₈N₆O₄S
• Molecular Weight: 554.714
• Mol file: 1446250-90-3.mol

Synonyms:

Chemical Property of C₂₈H₃₈N₆O₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₃₈N₆O₄S

There total 7 articles about C₂₈H₃₈N₆O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-diaminobenzoic acid methyl ester (107582-20-7) → C28H38N6O4S (1446250-90-3)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride / water / Reflux

2: hydrogenchloride / water / Reflux

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2013.05.018

Reference yield:

4-methanesulfonylpiperazine (55276-43-2) → C28H38N6O4S (1446250-90-3)

Guidance literature:

Multi-step reaction with 4 steps

1: ethanol

2: ethanol / Reflux

3: trifluoroacetic acid / dichloromethane

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2013.05.018

Reference yield:

rac-1-methylsulfonyl-4-(oxiranylmethyl)piperazine (1339114-58-7) → C28H38N6O4S (1446250-90-3)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol / Reflux

2: trifluoroacetic acid / dichloromethane

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2013.05.018

upstream raw materials:

C₁₄H₃₀N₄O₃S

2-Phenyl-4-benzimidazolylcarboxylic acid

2,3-diaminobenzoic acid methyl ester

4-methanesulfonylpiperazine