Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

Base Information

Chemical Name:Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2
CAS No.:200960-40-3
Molecular Formula:C₅₂H₄₈Cl₄P₄Re₂
Molecular Weight:1311.07
Hs Code.:

Re<sub>2</sub>Cl<sub>4</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2

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Chemical Property of Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

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Technology Process of Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

There total 2 articles about Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 55333-37-4,199454-40-5
Re₂Cl₄(P(CH₃)3)4

: 58298-35-4,200960-40-3,114720-23-9
Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

Guidance literature:: With C₂H₄(P(C₆H₅)2)2; In butan-1-ol; N2-atmosphere; refluxing (48 h, pptn.); filtration, washing (BuOH, Et2O), drying (vac.);

Reference yield:

: Re₂(OOCCH₃)Cl₄(P(C₆H₅)3)2

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: trans-dioxobis(1,2-bis(diphenylphosphino)ethane)rhenium(V)chloride

: 58298-35-4,200960-40-3,114720-23-9
Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

Guidance literature:: In dichloromethane; mixt. of Re-complex and ligand was stirred in CH2Cl2 at room temp. for 8 h under N2; dissolved in CH2Cl2, Et2O was diffused into soln., sepd.;
DOI:10.1039/b005975g