2',2-di-iodo-4,4,4''',6'-tetramethoxy-m-quaterphenyl

Base Information

Chemical Name:2',2-di-iodo-4,4,4''',6'-tetramethoxy-m-quaterphenyl
CAS No.:84389-91-3
Molecular Formula:C₂₈H₂₄I₂O₄
Molecular Weight:678.305
Hs Code.:

Synonyms:

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Chemical Property of 2',2-di-iodo-4,4,4''',6'-tetramethoxy-m-quaterphenyl

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Technology Process of 2',2-di-iodo-4,4,4''',6'-tetramethoxy-m-quaterphenyl

There total 1 articles about 2',2-di-iodo-4,4,4''',6'-tetramethoxy-m-quaterphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84251-63-8
2',2-diamino-4,4,4',6'-tetramethoxy-m-quaterphenyl

: 84389-91-3
2',2-di-iodo-4,4,4''',6'-tetramethoxy-m-quaterphenyl

Guidance literature:: With hydrogenchloride; potassium iodide; sodium iodide; mercury(II) iodide; sodium nitrite; Yield given. Multistep reaction;

Reference yield:

: 84389-91-3
2',2-di-iodo-4,4,4''',6'-tetramethoxy-m-quaterphenyl

: 3,5,7-trimethoxy-4,6-bis(4-methoxyphenyl)dibenzophosphole 5-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) BuLi, 2.) phosphorus trichloride / 1) THF, hexane, -78 deg C, 3.5 h; 2) THF, hexane, -78 deg C, 2.5 h

2: aq. sodium hydroxide, 30 percent hydrogen peroxide / Ambient temperature

3: diethyl ether; CH₂Cl₂

With sodium hydroxide; n-butyllithium; dihydrogen peroxide; phosphorus trichloride; In diethyl ether; dichloromethane;

Reference yield:

: 84389-91-3
2',2-di-iodo-4,4,4''',6'-tetramethoxy-m-quaterphenyl

: 5-Chloro-3,7-dimethoxy-4,6-bis-(4-methoxy-phenyl)-5H-dibenzophosphole

Guidance literature:: With n-butyllithium; phosphorus trichloride; Multistep reaction; 1) THF, hexane, -78 deg C, 3.5 h; 2) THF, hexane, -78 deg C, 2.5 h;