Technology Process of C58H92O9Si2
There total 12 articles about C58H92O9Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: NaHDMS / tetrahydrofuran / 2 h / -78 °C
1.2: 80 percent / tetrahydrofuran / -78 - -20 °C
2.1: 92 percent / LiOH*H2O; aq. H2O2 / tetrahydrofuran / 2 h / 20 °C
3.1: 96 percent / H2; K2CO3 / Pd/C / methanol / 0.83 h
4.1: EDC; DMAP / dimethylformamide / 12 h / 50 °C
With
dmap; lithium hydroxide; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.07.182
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 96 percent / H2; K2CO3 / Pd/C / methanol / 0.83 h
2: EDC; DMAP / dimethylformamide / 12 h / 50 °C
With
dmap; hydrogen; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide;
palladium on activated charcoal;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.07.182
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 92 percent / LiOH*H2O; aq. H2O2 / tetrahydrofuran / 2 h / 20 °C
2: 96 percent / H2; K2CO3 / Pd/C / methanol / 0.83 h
3: EDC; DMAP / dimethylformamide / 12 h / 50 °C
With
dmap; lithium hydroxide; hydrogen; dihydrogen peroxide; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.07.182
