Methanol, (dimethyl-1-naphthalenylsilyl)-, benzoate

Base Information

Chemical Name:Methanol, (dimethyl-1-naphthalenylsilyl)-, benzoate
CAS No.:137847-48-4
Molecular Formula:C₁₉H₁₈O₂Si
Molecular Weight:306.436
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanol, (dimethyl-1-naphthalenylsilyl)-, benzoate

Chemical Property:

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Technology Process of Methanol, (dimethyl-1-naphthalenylsilyl)-, benzoate

There total 5 articles about Methanol, (dimethyl-1-naphthalenylsilyl)-, benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90-11-9
1-Bromonaphthalene

: 137847-48-4
(Benzoyloxy)dimethyl(1-naphthyl)silan

Guidance literature:: Multi-step reaction with 5 steps

1: 1) Mg / 1) toluene, Et₂O, 2) 20h, reflux

2: 85 percent / dimethylformamide / 3 h / Heating

3: 67 percent / LiAlH₄ / diethyl ether / 6 h / Heating

4: 81 percent / NEt₃ / petroleum ether / 20 h / Ambient temperature

5: neat (no solvent) / 134.9 °C / lgA, E_A, ΔH(excit.), ΔS(excit.), ΔG(excit.), Δ_rH

With lithium aluminium tetrahydride; magnesium; triethylamine; In diethyl ether; N,N-dimethyl-formamide; Petroleum ether;

Reference yield:

: 137847-35-9
(Hydroxymethyl)methyl(1-naphthyl)silan

: 137847-48-4
(Benzoyloxy)dimethyl(1-naphthyl)silan

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NEt₃ / petroleum ether / 20 h / Ambient temperature

2: neat (no solvent) / 134.9 °C / lgA, E_A, ΔH(excit.), ΔS(excit.), ΔG(excit.), Δ_rH

With triethylamine; In Petroleum ether;

Reference yield:

: 137847-33-7
(Chlormethyl)methoxymethyl(1-naphthyl)silan

: 137847-48-4
(Benzoyloxy)dimethyl(1-naphthyl)silan

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / dimethylformamide / 3 h / Heating

2: 67 percent / LiAlH₄ / diethyl ether / 6 h / Heating

3: 81 percent / NEt₃ / petroleum ether / 20 h / Ambient temperature

4: neat (no solvent) / 134.9 °C / lgA, E_A, ΔH(excit.), ΔS(excit.), ΔG(excit.), Δ_rH

With lithium aluminium tetrahydride; triethylamine; In diethyl ether; N,N-dimethyl-formamide; Petroleum ether;