Technology Process of C37H52O3S
There total 7 articles about C37H52O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 92 percent / 1.33 h / 180 - 185 °C / base-washed flask
2: 92 percent / LiAlH4
3: pyridine / 5 h / 0 °C
4: 5.805 g / 1.1M ethanolic NaOEt / 1 h / Heating
5: 83 percent / bis(trimethylsilyl) peroxide / benzene / 24 h / Heating
With
lithium aluminium tetrahydride; bis-trimethylsilanyl peroxide; sodium ethanolate;
In
pyridine; benzene;
DOI:10.1039/P19830001783
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 81 percent / Hg(II)
2: 92 percent / 1.33 h / 180 - 185 °C / base-washed flask
3: 92 percent / LiAlH4
4: pyridine / 5 h / 0 °C
5: 5.805 g / 1.1M ethanolic NaOEt / 1 h / Heating
6: 83 percent / bis(trimethylsilyl) peroxide / benzene / 24 h / Heating
With
lithium aluminium tetrahydride; bis-trimethylsilanyl peroxide; mercury ion; sodium ethanolate;
In
pyridine; benzene;
DOI:10.1039/P19830001783
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / 5 h / 0 °C
2: 5.805 g / 1.1M ethanolic NaOEt / 1 h / Heating
3: 83 percent / bis(trimethylsilyl) peroxide / benzene / 24 h / Heating
With
bis-trimethylsilanyl peroxide; sodium ethanolate;
In
pyridine; benzene;
DOI:10.1039/P19830001783
