2-bromo-1,2-diphenylethyl nitrate

Base Information

• Chemical Name: 2-bromo-1,2-diphenylethyl nitrate
• CAS No.: 64342-52-5
• Molecular Formula: C₁₄H₁₂BrNO₃
• Molecular Weight: 322.158
• Mol file: 64342-52-5.mol

Synonyms:

Chemical Property of 2-bromo-1,2-diphenylethyl nitrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-bromo-1,2-diphenylethyl nitrate

There total 4 articles about 2-bromo-1,2-diphenylethyl nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-1,2-diphenyl-ethene (103-30-0) → 2-bromo-1,2-diphenylethyl nitrate (64342-52-5,64342-55-8) + 2-bromo-1,2-diphenylethyl nitrate (64342-52-5,64342-55-8)

Guidance literature:

With N-Bromosuccinimide; copper(II) nitrate trihydrate; In 1,4-dioxane; at 80 ℃; for 1h; Overall yield = 73 %; Overall yield = 70.7 mg; regioselective reaction;

DOI:10.1002/adsc.201900016

Reference yield:

(E)-1,2-diphenyl-ethene (103-30-0) → 2-bromo-1,2-diphenylethyl nitrate (64342-52-5,64342-55-8) + 2-bromo-1,2-diphenylethyl nitrate (64342-52-5,64342-55-8)

Guidance literature:

With N-Bromosuccinimide; copper(II) nitrate trihydrate; In 1,4-dioxane; at 80 ℃; for 1h; Overall yield = 73 %; Overall yield = 70.7 mg; regioselective reaction;

DOI:10.1002/adsc.201900016

Reference yield:

cis-stilben (645-49-8) → 2-bromo-1,2-diphenylethyl nitrate (64342-52-5,64342-55-8)

Guidance literature:

With pyridine; bromine; silver nitrate; In chloroform;

upstream raw materials:

(E)-1,2-diphenyl-ethene

cis-stilben