2-methyl-3-(2-methylpropyl)quinazolin-4(3H)-one

Base Information

• Chemical Name: 2-methyl-3-(2-methylpropyl)quinazolin-4(3H)-one
• CAS No.: 5784-51-0
• Molecular Formula: C₃₃H₂₅N₃O₃
• Molecular Weight: 511.58

Synonyms:4,7-Methano-1H-isoindole-1,3(2H)-dione,3a,4,7,7a-tetrahydro-5-(hydroxyphenyl-2-pyridinylmethyl)-8-(phenyl-2-pyridinylmethylene)-,[3aa,4b,5(R*),7b,7aa,8E]-(?à)-;5-Norbornene-2,3-dicarboximide, 5-(a-hydroxy-a-2-pyridylbenzyl)-7-(a-2-pyridylbenzylidene)-, trans-exo-threo- (8CI)

Chemical Property of 2-methyl-3-(2-methylpropyl)quinazolin-4(3H)-one

Chemical Property:

• Vapor Pressure: 9.85E-05mmHg at 25°C
• Boiling Point: 338.4°Cat760mmHg
• Flash Point: 158.5°C
• Density: 1.1g/cm³

Purity/Quality:

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Technology Process of 2-methyl-3-(2-methylpropyl)quinazolin-4(3H)-one

There total 1 articles about 2-methyl-3-(2-methylpropyl)quinazolin-4(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ [5-(α-hydroxy-α-2-pyridylbenzyl)-7-(α-2-pyridylbenzylidene)-5-norbornene-2,3-dicarboximide] (991-42-4,5779-10-2,5779-11-3,5779-12-4,5779-37-3,5784-49-6,5784-50-9,5784-51-0,5818-01-9)

Guidance literature:

2-<α-Hydroxy-α-(2'pyridyl)-benzyl>-6-phenyl-6-(2'-pyridyl)-fulven (geom. Isomerengem.), 1. N-Carbamoylmaleinimid, 2. HCl;

Reference yield: 71.0%

chloromethyl benzoate (5335-05-7) + [5-(α-hydroxy-α-2-pyridylbenzyl)-7-(α-2-pyridylbenzylidene)-5-norbornene-2,3-dicarboximide] (991-42-4,5779-10-2,5779-11-3,5779-12-4,5779-37-3,5784-49-6,5784-50-9,5784-51-0,5818-01-9) → N-benzoyloxymethyl-5-(α-hydroxy-α-2-pyridylbenzyl)-7-(α-2-pyridylbenzylidene)-5-norbornene-2,3-dicarboximide

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

DOI:10.1016/j.bmc.2012.05.014

Reference yield: 65.0%

chloromethyl 4-methoxybenzoic acid (75447-66-4) + [5-(α-hydroxy-α-2-pyridylbenzyl)-7-(α-2-pyridylbenzylidene)-5-norbornene-2,3-dicarboximide] (991-42-4,5779-10-2,5779-11-3,5779-12-4,5779-37-3,5784-49-6,5784-50-9,5784-51-0,5818-01-9) → 5-(α-hydroxy-α-2-pyridylbenzyl)-N-p-methoxybenzoyloxymethyl-7-(α-2-pyridylbenzylidene)-5-norbornene-2,3-dicarboximide

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

DOI:10.1016/j.bmc.2012.05.014

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