O[SbPh₂W(CO)5]2

Base Information

Chemical Name:O[SbPh₂W(CO)5]2
CAS No.:155230-97-0
Molecular Formula:C₃₄H₂₀O₁₁Sb₂W₂
Molecular Weight:1215.73
Hs Code.:

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Chemical Property of O[SbPh₂W(CO)5]2

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Technology Process of O[SbPh₂W(CO)5]2

There total 2 articles about O[SbPh₂W(CO)5]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 155230-90-3
[W(CO)5(Ph₂SbCl)]

: 1310-73-2
sodium hydroxide

: 155230-97-0
O[SbPh₂W(CO)5]2

Guidance literature:: In diethyl ether; water; byproducts: NaCl, H2O; (Ar); dropwise addn. of a soln. of W complex in Et2O to a soln. of NaOH in water, stirring at room temp. for 2 h; sepn., extn. of aq. phase with Et2O, drying org. phase with Na2SO4, filtration, cooling to -28°C;
DOI:10.1002/zaac.200800104

Reference yield: 47.0%

: 14040-11-0
tungsten hexacarbonyl

: 7065-22-7
bis(diphenylantimony)oxide

: 155230-97-0
O[SbPh₂W(CO)5]2

Guidance literature:: In tetrahydrofuran; byproducts: CO; Irradiation (UV/VIS); soln. of metal carbonyl in THF is irradiated at -20°C and dropped to a soln. of stibane, mixt. is allowed to warm to room temp. with stirring for 20 h (N2); solvent is removed under reduced pressure, residue is recrystd. from petroleum ether/CH2Cl2 at -30°C, ppt. is washed with petroleum ether and dried at 0.1 Torr and 30°C for several hours, molecular weigth detn., elem. anal.;