[Pd(N,N,N',N'-tetramethylethylenediamine)(C₆F₅)(OH)]

Base Information

Chemical Name:[Pd(N,N,N',N'-tetramethylethylenediamine)(C₆F₅)(OH)]
CAS No.:552320-19-1
Molecular Formula:C₁₂H₁₇F₅N₂OPd
Molecular Weight:406.692
Hs Code.:

[Pd(N,N,N',N'-tetramethylethylenediamine)(C<sub>6</sub>F<sub>5</sub>)(OH)]

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Pd(N,N,N',N'-tetramethylethylenediamine)(C₆F₅)(OH)]

Chemical Property:

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Technology Process of [Pd(N,N,N',N'-tetramethylethylenediamine)(C₆F₅)(OH)]

There total 1 articles about [Pd(N,N,N',N'-tetramethylethylenediamine)(C₆F₅)(OH)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 552320-52-2
[Pd(N,N,N',N'-tetramethylethylenediamine)(pentafluorophenyl)(acetone)]ClO₄

: potassium hydroxide

: 552320-19-1
[Pd(N,N,N',N'-tetramethylethylenediamine)(C₆F₅)(OH)]

Guidance literature:: In methanol; KOH added to soln. of Pd complex in MeOH, stirred for 1 h; soln. evapd. to dryness in vacuo, residue treated with CH2Cl2, ppt. removed by filtration, filtrate concd., hexane added, ppt. filtered off and dried in air; elem. anal.;
DOI:10.1021/ic0300058

Reference yield: 92.0%

: 541-59-3,25721-74-8
maleiimide

: 552320-19-1
[Pd(N,N,N',N'-tetramethylethylenediamine)(C₆F₅)(OH)]

: 858977-78-3
[Pd(N,N,N',N'-tetramethylethylenediamine)(C₆F₅)(maleimidato)]

Guidance literature:: In toluene; byproducts: H2O; ligand added to Pd complex in toluene, stirred for 90 min; concd. (vac.), pptd. (hexane), filtered, air-dried; elem. anal.;
DOI:10.1039/b503101j

Reference yield: 87.0%

: 552320-19-1
[Pd(N,N,N',N'-tetramethylethylenediamine)(C₆F₅)(OH)]

: 7446-09-5,12143-17-8,89125-89-3
sulfur dioxide

: 67-63-0,8013-70-5
isopropyl alcohol

: [Pd(N,N,N',N'-tetramethylethylenediamine)(C₆F₅)(SO₂O(i)Pr)]

Guidance literature:: In isopropyl alcohol; bubbling SO2 through a soln. of palladium complex in isopropanol at roomtemp. for 10 min; evapn., addn. of ether-hexane, filtration, air drying; elem. anal.;
DOI:10.1039/b316697j