Technology Process of 3-bromo-4-((2-ethylhexyl)oxy)phenol
There total 5 articles about 3-bromo-4-((2-ethylhexyl)oxy)phenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium hydroxide / dimethyl sulfoxide / 50 °C / Inert atmosphere
2: triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere
3: potassium acetate; bromine / acetic acid / 50 °C / Inert atmosphere
4: sodium hydroxide; water / tert-butyl alcohol / Inert atmosphere; Reflux
With
water; bromine; potassium acetate; triethylamine; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; acetic acid; dimethyl sulfoxide; tert-butyl alcohol;
1: |Williamson Ether Synthesis;
DOI:10.1021/jo501266g
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium acetate; bromine / acetic acid / 50 °C / Inert atmosphere
2: sodium hydroxide; water / tert-butyl alcohol / Inert atmosphere; Reflux
With
water; bromine; potassium acetate; sodium hydroxide;
In
acetic acid; tert-butyl alcohol;
DOI:10.1021/jo501266g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere
2: potassium acetate; bromine / acetic acid / 50 °C / Inert atmosphere
3: sodium hydroxide; water / tert-butyl alcohol / Inert atmosphere; Reflux
With
water; bromine; potassium acetate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; acetic acid; tert-butyl alcohol;
DOI:10.1021/jo501266g
