cis-(1,1-dimethyl-4-phenyl-1-silacyclohexa-2,4-diene) molybdenum⁽⁰⁾-dicarbonyl complex

Base Information

• Chemical Name: cis-(1,1-dimethyl-4-phenyl-1-silacyclohexa-2,4-diene) molybdenum⁽⁰⁾-dicarbonyl complex
• CAS No.: 73655-81-9
• Molecular Formula: C₂₈H₃₂MoO₂Si₂
• Molecular Weight: 552.672

Synonyms:

Chemical Property of cis-(1,1-dimethyl-4-phenyl-1-silacyclohexa-2,4-diene) molybdenum⁽⁰⁾-dicarbonyl complex

Chemical Property:

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Technology Process of cis-(1,1-dimethyl-4-phenyl-1-silacyclohexa-2,4-diene) molybdenum⁽⁰⁾-dicarbonyl complex

There total 1 articles about cis-(1,1-dimethyl-4-phenyl-1-silacyclohexa-2,4-diene) molybdenum⁽⁰⁾-dicarbonyl complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.8%

1,1-dimethyl-4-phenyl-1-silacyclohexa-2,4-diene (71759-82-5) + molybdenum hexacarbonyl (13939-06-5,199620-15-0) → cis-(1,1-dimethyl-4-phenyl-1-silacyclohexa-2,4-diene) molybdenum(0)-dicarbonyl complex (73655-81-9)

Guidance literature:

With acetonitrile; In methyl cyclohexane; (N2); Mo(CO)6 was refluxed for 16 h in acetonitrile, solvent was removed under reduced pressure, residue was refluxed with the silacyclohexadienederiv. in methylcyclohexane for 48 h; filtered soln. was evapd. in vac. to dryness, residue was treated with PE and filtered off, recrystn. from cyclohexane; elem. anal.;

DOI:10.1016/S0022-328X(00)90532-1

upstream raw materials:

1,1-dimethyl-4-phenyl-1-silacyclohexa-2,4-diene

molybdenum hexacarbonyl

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