Technology Process of C17H16N3OPS
There total 9 articles about C17H16N3OPS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine / 168 h / -30 - 20 °C
2: dihydrogen peroxide / diethyl ether
With
pyridine; dihydrogen peroxide;
In
diethyl ether;
DOI:10.1002/hc.20658
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydroxide / methanol / 2 h / 20 °C
2: ferrous(II) sulfate heptahydrate; ammonia; water / 2 h / 50 °C / Reflux
3: water / 0.5 h / Reflux
4: lithium aluminium tetrahydride / tetrahydrofuran / 2 h
5: pyridine / 168 h / -30 - 20 °C
6: dihydrogen peroxide / diethyl ether
With
pyridine; ferrous(II) sulfate heptahydrate; lithium aluminium tetrahydride; ammonia; water; dihydrogen peroxide; sodium hydroxide;
In
tetrahydrofuran; methanol; diethyl ether; water;
DOI:10.1002/hc.20658
- Guidance literature:
-
Multi-step reaction with 9 steps
1: hydrogenchloride / water / 4 h / 20 °C
2: ethanol / 0.5 h / Reflux
3: hydrogenchloride; water / 1 h / Reflux
4: sodium hydroxide / methanol / 2 h / 20 °C
5: ferrous(II) sulfate heptahydrate; ammonia; water / 2 h / 50 °C / Reflux
6: water / 0.5 h / Reflux
7: lithium aluminium tetrahydride / tetrahydrofuran / 2 h
8: pyridine / 168 h / -30 - 20 °C
9: dihydrogen peroxide / diethyl ether
With
pyridine; hydrogenchloride; ferrous(II) sulfate heptahydrate; lithium aluminium tetrahydride; ammonia; water; dihydrogen peroxide; sodium hydroxide;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; water;
DOI:10.1002/hc.20658