1,4-bis[bis(trimethylsilyl)methyldiphenylstannylmethyldimethylsilyl]benzene

Base Information

Chemical Name:1,4-bis[bis(trimethylsilyl)methyldiphenylstannylmethyldimethylsilyl]benzene
CAS No.:503815-76-7
Molecular Formula:C₅₀H₇₈Si₆Sn₂
Molecular Weight:1085.1
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-bis[bis(trimethylsilyl)methyldiphenylstannylmethyldimethylsilyl]benzene

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Technology Process of 1,4-bis[bis(trimethylsilyl)methyldiphenylstannylmethyldimethylsilyl]benzene

There total 2 articles about 1,4-bis[bis(trimethylsilyl)methyldiphenylstannylmethyldimethylsilyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 404875-11-2
1,4-bis((triphenylstannylmethyl)dimethylsilyl)benzene

: 503815-76-7
1,4-bis[bis(trimethylsilyl)methyldiphenylstannylmethyldimethylsilyl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: diethyl ether

In diethyl ether; dichloromethane;
DOI:10.1021/om020749d

Reference yield:

: 503815-75-6
1,4-bis((iododimethylstannylmethyl)dimethylsilyl)benzene

: 41823-71-6
bis(trimethylsilyl)methyllithium

: 503815-76-7
1,4-bis[bis(trimethylsilyl)methyldiphenylstannylmethyldimethylsilyl]benzene

Guidance literature:: In diethyl ether; byproducts: LiI; addn. of soln. of 1,4-bis(iododiphenylstannylmethyldimethylsilyl)benzenein Et2O to soln. of LiCH(SiMe3)2 in Et2O for 40 min at room temp.; stir ring overnight; addn. of satd. NH4Cl; sepn. of org. layer; washing twice with water, drying over Na2SO4; filtration, evapn. in vac., keeping at 130°C and10**-3 Torr for 1 h;
DOI:10.1021/om020749d

Reference yield: 51.0%

: 503815-76-7
1,4-bis[bis(trimethylsilyl)methyldiphenylstannylmethyldimethylsilyl]benzene

: mercury dichloride

: 503815-73-4
1,4-bis[bis(trimethylsilyl)methyldichlorostannylmethyldimethylsilyl]benzene

Guidance literature:: In acetone; byproducts: PhHgCl; addn. dropwise soln. of HgCl2 in acetone to magnetically stirred and cooled (0°C) soln. of ((SiMe3)2CHPh2SnCH2SiMe2)2C6H4 in acetone for 30 min; stirring for 7 days; removal of acetone in vac.; addn. of hexane; reflux for 10 min; filtration, evapn. of org. solvent in vac., recrystn. from CHCl3; elem. anal.;
DOI:10.1021/om020749d