trans-Pd(PPh₃)2(o-MeOC₆H₄)(I)

Base Information

Chemical Name:trans-Pd(PPh₃)2(o-MeOC₆H₄)(I)
CAS No.:180891-47-8
Molecular Formula:C₄₃H₃₇IOP₂Pd
Molecular Weight:865.038
Hs Code.:

trans-Pd(PPh<sub>3</sub>)2(o-MeOC<sub>6</sub>H<sub>4</sub>)(I)

Synonyms:

Suppliers and Price of trans-Pd(PPh₃)2(o-MeOC₆H₄)(I)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trans-Pd(PPh₃)2(o-MeOC₆H₄)(I)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trans-Pd(PPh₃)2(o-MeOC₆H₄)(I)

There total 2 articles about trans-Pd(PPh₃)2(o-MeOC₆H₄)(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1271-03-0
allyl(cyclopentadiene)palladium(II)

: 529-28-2
4-iodoanisol

: 603-35-0
triphenylphosphine

: 180891-47-8
(2-methoxyphenyl)Pd(P(C₆H₅)3)2I

Guidance literature:: In dichloromethane; Ar-atmosphere; stirring (room temp., 5 - 15 min); filtering (PTFE membrane), crystn. on concg. and hexane addn. (-30°C, overnight), filtering, drying (vac.); elem. anal.;
DOI:10.1021/om9602567

Reference yield: 80.0%

: 14221-01-3
tetrakis(triphenylphosphine) palladium⁽⁰⁾

: 529-28-2
4-iodoanisol

: 180891-47-8
trans-Pd(PPh₃)2(o-MeOC₆H₄)(I)

Guidance literature:: In toluene; under N2; at room temp.; o-AnI added to suspn. of Pd(PPh3)4 in toluene; suspn. stirred for 1 h and filtered; solid washed with Et2O;
DOI:10.1021/om030144x

Reference yield: 63.0%

: 180891-47-8
trans-Pd(PPh₃)2(o-MeOC₆H₄)(I)

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 586945-04-2
Pd(dppe)(o-MeOC₆H₄)(I)

Guidance literature:: In toluene; under N2; at room temp.; soln. of dppe in toluene added to soln. of the Pd complex in toluene; suspn. stirred for 45 min; toluene removed in vacuo; petroleum ether added; soln. stirred for 12 h;solid collected on fine frit and dried; sample for anal. recrystd. from CHCl3/ether at -25 °C; elem. anal.;
DOI:10.1021/om030144x