Technology Process of BF4(1-)*C17H25N4O(1+)
There total 6 articles about BF4(1-)*C17H25N4O(1+) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrazine hydrate / acetonitrile / 8 h / 80 °C
2: diisopropyl-carbodiimide / acetonitrile / 8 h / 20 °C / Inert atmosphere
3: trifluoroacetic acid / dichloromethane
With
hydrazine hydrate; trifluoroacetic acid; diisopropyl-carbodiimide;
In
dichloromethane; acetonitrile;
DOI:10.1080/00397910903013697
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium tetrafluoroborate / acetonitrile / 72 h / 80 °C
2: hydrazine hydrate / acetonitrile / 8 h / 80 °C
3: diisopropyl-carbodiimide / acetonitrile / 8 h / 20 °C / Inert atmosphere
4: trifluoroacetic acid / dichloromethane
With
sodium tetrafluoroborate; hydrazine hydrate; trifluoroacetic acid; diisopropyl-carbodiimide;
In
dichloromethane; acetonitrile;
DOI:10.1080/00397910903013697
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diisopropyl-carbodiimide / acetonitrile / 8 h / 20 °C / Inert atmosphere
2: trifluoroacetic acid / dichloromethane
With
trifluoroacetic acid; diisopropyl-carbodiimide;
In
dichloromethane; acetonitrile;
DOI:10.1080/00397910903013697