NiCl₂((S)a(R,R)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine)

Base Information

• Chemical Name: NiCl₂((S)a(R,R)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine)
• CAS No.: 156952-40-8
• Molecular Formula: C₄₈H₄₆Cl₂NiO₂P₂
• Molecular Weight: 846.436

Synonyms:

Chemical Property of NiCl₂((S)a(R,R)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of NiCl₂((S)a(R,R)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine)

There total 3 articles about NiCl₂((S)a(R,R)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

nickel(II) chloride hexahydrate + (S)a(R,R)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine (156629-38-8,156714-48-6,158112-28-8,158112-26-6,158112-27-7,156714-49-7) → NiCl2((S)a(R,R)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine) (156952-40-8,158112-43-7,158112-41-5,158112-42-6)

Guidance literature:

In ethanol; dichloromethane; addn. of NiCl2*6H2O in ethanol to a CH2Cl2 soln. of ligand, allowed to stand for 12 h; ppt. collected, dried in vac.;

Reference yield: 83.0%

nickel(II) chloride hexahydrate + (S)a(S,S)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine (156714-48-6,158112-28-8,156629-38-8,156714-49-7,158112-27-7,158112-26-6) → NiCl2((S)a(S,S)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine) (158112-42-6,158112-41-5,158112-43-7,156952-40-8)

Guidance literature:

In ethanol; dichloromethane; addn. of NiCl2*6H2O in ethanol to a CH2Cl2 soln. of ligand, allowed to stand for 12 h; ppt. collected, dried in vac.;

Reference yield: 77.0%

nickel(II) chloride hexahydrate + (S)a(S,R)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine (156629-38-8,158112-27-7,158112-26-6,156714-48-6,158112-28-8,156714-49-7) → NiCl2((S)a(S,R)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine) (156952-40-8,158112-43-7,158112-42-6,158112-41-5)

Guidance literature:

In ethanol; dichloromethane; addn. of NiCl2*6H2O in ethanol to a CH2Cl2 soln. of ligand, allowed to stand for 12 h; ppt. collected, dried in vac.; elem. anal.;

upstream raw materials:

(S)a(S,R)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine

(S)a(S,S)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine

(S)a(R,R)P-12,13,14,15,16,17,22,23,24,25,26,27-dodecahydro-17,22-diphenylbenzo{m}dinaphtho{2,1-b:1',2'-d}{1,6,12,15}dioxadiphosphacycloeicosine

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