Technology Process of C27H30O6
There total 7 articles about C27H30O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride; water; acetic acid;
for 0.5h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium aluminium tetrahydride
2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone
3.1: sodium hydride / 1,2-dimethoxyethane; paraffin oil / 0.17 h
3.2: 3 h / Reflux
4.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -10 °C / Inert atmosphere
4.2: 2 h / -78 - 20 °C
5.1: hydrogenchloride; water; acetic acid / 0.5 h / Reflux
With
hydrogenchloride; lithium aluminium tetrahydride; n-butyllithium; water; sodium hydride; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
1,2-dimethoxyethane; diethyl ether; hexane; paraffin oil;
3.1: Wittig-Horner reaction / 3.2: Wittig-Horner reaction;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -10 °C / Inert atmosphere
1.2: 2 h / -78 - 20 °C
2.1: hydrogenchloride; water; acetic acid / 0.5 h / Reflux
With
hydrogenchloride; n-butyllithium; water; acetic acid;
In
diethyl ether; hexane;