C₃₃H₂₅N₂O₂⁽¹⁺⁾*I^(1-)

Base Information

Chemical Name:C₃₃H₂₅N₂O₂⁽¹⁺⁾*I^(1-)
CAS No.:1354558-68-1
Molecular Formula:C₃₃H₂₅N₂O₂*I
Molecular Weight:608.478
Hs Code.:

C<sub>33</sub>H<sub>25</sub>N<sub>2</sub>O<sub>2</sub><sup>(1+)</sup>*I<sup>(1-)</sup>

Synonyms:

Suppliers and Price of C₃₃H₂₅N₂O₂⁽¹⁺⁾*I^(1-)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₂₅N₂O₂⁽¹⁺⁾*I^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₂₅N₂O₂⁽¹⁺⁾*I^(1-)

There total 13 articles about C₃₃H₂₅N₂O₂⁽¹⁺⁾*I^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354694-98-6
CF₃O₃S^(1-)*C₃₃H₂₅N₂O₂⁽¹⁺⁾

: 1354558-68-1
C₃₃H₂₅N₂O₂⁽¹⁺⁾*I^(1-)

Guidance literature:: With sodium iodide; In acetone; at 20 ℃; for 2h;
DOI:10.1039/c1ob06780j

Reference yield:

: 7-phenyl-2,3-dihydro-1H-inden-1-one

: 1354558-68-1
C₃₃H₂₅N₂O₂⁽¹⁺⁾*I^(1-)

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

2.1: Amberlyst 15 / hexane / 3 h / 0 - 20 °C / Reflux

3.1: C₃₈H₄₂ClMnN₂O₄; 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / -78 °C

3.2: -78 °C

4.1: sodium azide; ammonium chloride / ethanol; water / 2 h / Reflux

5.1: palladium 10% on activated carbon; hydrogen / methanol / 0.33 h

6.1: acetic acid / tetrahydrofuran / 16 h / 90 °C

7.1: thionyl chloride / toluene / 16 h / 90 °C

8.1: sodium hydroxide / tetrahydrofuran; ethanol / 3 h / 90 °C

9.1: dichloromethane / 2 h / 20 °C / Darkness

10.1: sodium iodide / acetone / 2 h / 20 °C

With sodium tetrahydroborate; thionyl chloride; sodium azide; palladium 10% on activated carbon; C₃₈H₄₂ClMnN₂O₄; hydrogen; ammonium chloride; acetic acid; 4-methylmorpholine N-oxide; sodium iodide; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; acetone; toluene;
DOI:10.1039/c1ob06780j

Reference yield:

: 868374-23-6
3-oxo-2,3-dihydro-1H-inden-4-yl trifluoromethanesulfonate

: 1354558-68-1
C₃₃H₂₅N₂O₂⁽¹⁺⁾*I^(1-)

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / Inert atmosphere; Reflux

2.1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

3.1: Amberlyst 15 / hexane / 3 h / 0 - 20 °C / Reflux

4.1: C₃₈H₄₂ClMnN₂O₄; 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / -78 °C

4.2: -78 °C

5.1: sodium azide; ammonium chloride / ethanol; water / 2 h / Reflux

6.1: palladium 10% on activated carbon; hydrogen / methanol / 0.33 h

7.1: acetic acid / tetrahydrofuran / 16 h / 90 °C

8.1: thionyl chloride / toluene / 16 h / 90 °C

9.1: sodium hydroxide / tetrahydrofuran; ethanol / 3 h / 90 °C

10.1: dichloromethane / 2 h / 20 °C / Darkness

11.1: sodium iodide / acetone / 2 h / 20 °C

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; sodium azide; palladium 10% on activated carbon; C₃₈H₄₂ClMnN₂O₄; hydrogen; sodium carbonate; ammonium chloride; acetic acid; 4-methylmorpholine N-oxide; sodium iodide; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; acetone; toluene;
DOI:10.1039/c1ob06780j