Silane, [(2-methyl-1-cyclohexen-1-yl)oxy]tris(1-methylethyl)-

Base Information

Chemical Name:Silane, [(2-methyl-1-cyclohexen-1-yl)oxy]tris(1-methylethyl)-
CAS No.:137897-39-3
Molecular Formula:C16H32OSi
Molecular Weight:268.515
Hs Code.:
DSSTox Substance ID:DTXSID50454392
Nikkaji Number:J694.313F
Wikidata:Q82275892
Mol file:137897-39-3.mol

Synonyms:137897-39-3;Silane, [(2-methyl-1-cyclohexen-1-yl)oxy]tris(1-methylethyl)-;DTXSID50454392;2-Methyl-1-(triisopropylsilyloxy)cyclohexene

Suppliers and Price of Silane, [(2-methyl-1-cyclohexen-1-yl)oxy]tris(1-methylethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, [(2-methyl-1-cyclohexen-1-yl)oxy]tris(1-methylethyl)-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:268.222242174
Heavy Atom Count:18
Complexity:280

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(CCCC1)O[Si](C(C)C)(C(C)C)C(C)C

Technology Process of Silane, [(2-methyl-1-cyclohexen-1-yl)oxy]tris(1-methylethyl)-

There total 3 articles about Silane, [(2-methyl-1-cyclohexen-1-yl)oxy]tris(1-methylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 583-60-8
2-Methylcyclohexanone

: 137897-39-3
2-methyl-1-triisopropylsilyl(oxy)-cyclohex-1-ene

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1016/0040-4020(95)00696-6

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 583-60-8
2-Methylcyclohexanone

: 137897-39-3
2-methyl-1-triisopropylsilyl(oxy)-cyclohex-1-ene

: 137897-41-7
6-methyl-1-triisopropylsilyl(oxy)-cyclohex-1-ene

Guidance literature:: triisopropylsilyl trifluoromethanesulfonate; 2-Methylcyclohexanone; With triethylamine; In dichloromethane; at 20 ℃; for 5.5h; Inert atmosphere;

With pyridine hydrochloride; In dichloromethane; at 20 ℃; for 1.5h; Overall yield = 84 %; Overall yield = 2.7 g; Inert atmosphere;
DOI:10.1021/jacs.6b06847

Reference yield:

: 137897-41-7
6-methyl-1-triisopropylsilyl(oxy)-cyclohex-1-ene

: 137897-39-3
2-methyl-1-triisopropylsilyl(oxy)-cyclohex-1-ene

Guidance literature:: With bis(trifluoromethanesulfonyl)amide; In dichloromethane; toluene; at -10 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.3762/bjoc.8.73