24-(t-butylcarbamoyl)-41-(cyclohexylamino)-8-(dec-9-en-1-yl)-7,10,26,41-tetraoxo-9,25-dioxa-13,29-dithia-6-azahentetracontan-40-yl stearate

Base Information

Chemical Name:24-(t-butylcarbamoyl)-41-(cyclohexylamino)-8-(dec-9-en-1-yl)-7,10,26,41-tetraoxo-9,25-dioxa-13,29-dithia-6-azahentetracontan-40-yl stearate
CAS No.:1609930-03-1
Molecular Formula:C₇₅H₁₃₉N₃O₉S₂
Molecular Weight:1291.08
Hs Code.:

24-(t-butylcarbamoyl)-41-(cyclohexylamino)-8-(dec-9-en-1-yl)-7,10,26,41-tetraoxo-9,25-dioxa-13,29-dithia-6-azahentetracontan-40-yl stearate

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Chemical Property of 24-(t-butylcarbamoyl)-41-(cyclohexylamino)-8-(dec-9-en-1-yl)-7,10,26,41-tetraoxo-9,25-dioxa-13,29-dithia-6-azahentetracontan-40-yl stearate

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Technology Process of 24-(t-butylcarbamoyl)-41-(cyclohexylamino)-8-(dec-9-en-1-yl)-7,10,26,41-tetraoxo-9,25-dioxa-13,29-dithia-6-azahentetracontan-40-yl stearate

There total 7 articles about 24-(t-butylcarbamoyl)-41-(cyclohexylamino)-8-(dec-9-en-1-yl)-7,10,26,41-tetraoxo-9,25-dioxa-13,29-dithia-6-azahentetracontan-40-yl stearate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 18971-59-0
1-pentylisonitrile

: 112-45-8
10-Undecenal

: 1609930-02-0
15-(t-butylcarbamoyl)-31-(cyclohexylcarbamoyl)-17,33-dioxo-16,32-dioxa-4,20-dithiapentacontan-1-oic acid

: 1609930-03-1
24-(t-butylcarbamoyl)-41-(cyclohexylamino)-8-(dec-9-en-1-yl)-7,10,26,41-tetraoxo-9,25-dioxa-13,29-dithia-6-azahentetracontan-40-yl stearate

Guidance literature:: In dichloromethane; at 20 ℃; for 15h;
DOI:10.1002/anie.201308960

Reference yield:

: 1609930-15-5
1-(cyclohexylamino)-1-oxododec-11-en-2-yl stearate

: 1609930-03-1
24-(t-butylcarbamoyl)-41-(cyclohexylamino)-8-(dec-9-en-1-yl)-7,10,26,41-tetraoxo-9,25-dioxa-13,29-dithia-6-azahentetracontan-40-yl stearate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,2-dimethoxy-2-phenylacetophenone / 1 h / 20 °C / UV-irradiation

2.1: dichloromethane / 0.17 h / 20 °C

2.2: 12 h / 20 °C

3.1: 2,2-dimethoxy-2-phenylacetophenone / 2 h / 20 °C / UV-irradiation

4.1: dichloromethane / 15 h / 20 °C

With 2,2-dimethoxy-2-phenylacetophenone; In dichloromethane; 2.1: |Passerini Condensation / 2.2: |Passerini Condensation / 4.1: |Passerini Condensation;
DOI:10.1002/anie.201308960

Reference yield:

: 57-11-4
stearic acid

: 1609930-03-1
24-(t-butylcarbamoyl)-41-(cyclohexylamino)-8-(dec-9-en-1-yl)-7,10,26,41-tetraoxo-9,25-dioxa-13,29-dithia-6-azahentetracontan-40-yl stearate

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane / 2 h / 20 °C

2.1: 2,2-dimethoxy-2-phenylacetophenone / 1 h / 20 °C / UV-irradiation

3.1: dichloromethane / 0.17 h / 20 °C

3.2: 12 h / 20 °C

4.1: 2,2-dimethoxy-2-phenylacetophenone / 2 h / 20 °C / UV-irradiation

5.1: dichloromethane / 15 h / 20 °C

With 2,2-dimethoxy-2-phenylacetophenone; In dichloromethane; 1.1: |Passerini Condensation / 3.1: |Passerini Condensation / 3.2: |Passerini Condensation / 5.1: |Passerini Condensation;
DOI:10.1002/anie.201308960