2,3,4,5-tetrafluorobenzyl N-tosyloxycarbamate

Base Information

Chemical Name:2,3,4,5-tetrafluorobenzyl N-tosyloxycarbamate
CAS No.:1374003-02-7
Molecular Formula:C₁₅H₁₁F₄NO₅S
Molecular Weight:393.316
Hs Code.:

Synonyms:

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Chemical Property of 2,3,4,5-tetrafluorobenzyl N-tosyloxycarbamate

Chemical Property:

Purity/Quality:

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Technology Process of 2,3,4,5-tetrafluorobenzyl N-tosyloxycarbamate

There total 2 articles about 2,3,4,5-tetrafluorobenzyl N-tosyloxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₆F₄N₂O₂

: 1374003-02-7
2,3,4,5-tetrafluorobenzyl N-tosyloxycarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole; hydroxylamine hydrochloride / acetonitrile / 16 h / 20 °C / Inert atmosphere

2: triethylamine / diethyl ether / 2 h / 20 °C / Inert atmosphere

With 1H-imidazole; hydroxylamine hydrochloride; triethylamine; In diethyl ether; acetonitrile;
DOI:10.1016/j.tet.2012.02.044

Reference yield:

: 53072-18-7
2,3,4,5-tetrafluorobenzyl alcohol

: 1374003-02-7
2,3,4,5-tetrafluorobenzyl N-tosyloxycarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 3 h / 20 °C / Inert atmosphere

2: 1H-imidazole; hydroxylamine hydrochloride / acetonitrile / 16 h / 20 °C / Inert atmosphere

3: triethylamine / diethyl ether / 2 h / 20 °C / Inert atmosphere

With 1H-imidazole; hydroxylamine hydrochloride; triethylamine; In diethyl ether; acetonitrile;
DOI:10.1016/j.tet.2012.02.044

Reference yield:

: 100-13-0
4-nitrostyrene

: 1374003-02-7
2,3,4,5-tetrafluorobenzyl N-tosyloxycarbamate

: C₁₆H₁₀F₄N₂O₄

: 1374003-10-7
C₁₆H₁₀F₄N₂O₄

Guidance literature:: With tetrakis(actonitrile)copper(I) hexafluorophosphate; (4R,4'R)-2,2'-(propane-2,2-diyl)bis(5,5-dimethyl-4-phenyl-4,5-dihydrooxazole); potassium carbonate; In acetonitrile; at 23 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.tet.2012.02.044