C₅H₅CoBrP(C₆H₅)3

Base Information

• Chemical Name: C₅H₅CoBrP(C₆H₅)3
• CAS No.: 80719-20-6
• Molecular Formula: C₂₃H₂₀BrCoP
• Molecular Weight: 466.283
• Mol file: 80719-20-6.mol

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Chemical Property of C₅H₅CoBrP(C₆H₅)3

Chemical Property:

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Technology Process of C₅H₅CoBrP(C₆H₅)3

There total 1 articles about C₅H₅CoBrP(C₆H₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

dibromo-bis-triphenylphosphine cobalt (14126-32-0) + cyclopentadienylthallium(I) → C5H5CoBrP(C6H5)3 (80719-20-6)

Guidance literature:

In tetrahydrofuran; Co complex dissolving in THF under N2, treating with CpTl, stirring for4 h at room temp., solid filtering off, heptane adding to the filtrate, concg., ppt. sepg., drying under high vacuum at 50°C for 3 h; identified by elem. anal.;

DOI:10.1021/ic00135a065

upstream raw materials:

dibromo-bis-triphenylphosphine cobalt