[iron(II)(η5-C5H5)(CO)2(1,3,5,7-tetraazaadamantane)]BPh4

Base Information

• Chemical Name: [iron(II)(η5-C5H5)(CO)2(1,3,5,7-tetraazaadamantane)]BPh4
• CAS No.: 1386412-70-9
• Molecular Formula: C₁₃H₁₇FeN₄O₂*C₂₄H₂₀B
• Molecular Weight: 636.384
• Mol file: 1386412-70-9.mol

Synonyms:

Chemical Property of [iron(II)(η5-C5H5)(CO)2(1,3,5,7-tetraazaadamantane)]BPh4

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of [iron(II)(η5-C5H5)(CO)2(1,3,5,7-tetraazaadamantane)]BPh4

There total 1 articles about [iron(II)(η5-C5H5)(CO)2(1,3,5,7-tetraazaadamantane)]BPh4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[iron(II)(η5-C5H5)(CO)2(1,3,5,7-tetraazaadamantane)](BF4) (1386412-78-7) + sodium tetraphenyl borate (143-66-8) → [iron(II)(η5-C5H5)(CO)2(1,3,5,7-tetraazaadamantane)]BPh4 (1386412-70-9)

Guidance literature:

In acetone; under N2 atm., acetone soln. of NaBPh4 added into soln. of Fe in acetone, mixt. stirred for 4 h; solvent removed under reduced pressure, extd. with CH2Cl2; Et2O added toextract, pptd., mixt. kept for 20 min, mother liquor syringed off, ppt washed (Et2O), dried under reduced pressure; elem. anal.;

DOI:10.1016/j.ica.2012.04.003

upstream raw materials:

[iron(II)(η5-C5H5)(CO)2(1,3,5,7-tetraazaadamantane)](BF4)

sodium tetraphenyl borate