2-trimethylsilyl-1-stibaphenalene

Base Information

Chemical Name:2-trimethylsilyl-1-stibaphenalene
CAS No.:354818-38-5
Molecular Formula:C₂₁H₂₁SbSi
Molecular Weight:423.233
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-trimethylsilyl-1-stibaphenalene

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Technology Process of 2-trimethylsilyl-1-stibaphenalene

There total 2 articles about 2-trimethylsilyl-1-stibaphenalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 73046-27-2
dibromophenylantimony

: 354818-37-4
(Z)-1-bromo-2-[1-(8-bromonaphthyl)]-1-trimethylsilylethene

: 354818-38-5
2-trimethylsilyl-1-stibaphenalene

Guidance literature:: With tBuLi; In diethyl ether; tBuLi at -80°C for 1 h and PhSbBr2 at -80°C for 4 h added to organic reagent; elem. anal.;
DOI:10.1246/cl.2001.554

Reference yield:

: 73046-27-2
dibromophenylantimony

: (Z)-1-bromo-2-(1-naphthyl)-1-trimethylsilylethene

: 354818-38-5
2-trimethylsilyl-1-stibaphenalene

Guidance literature:: With tBuLi; In diethyl ether; tBuLi at -80°C for 1 h and PhSbBr2 at -80°C for 4 h added to organic reagent;
DOI:10.1246/cl.2001.554

Reference yield: 61.0%

: 354818-38-5
2-trimethylsilyl-1-stibaphenalene

: 354818-35-2
1-phenyl-1-stibaphenarene

Guidance literature:: With TBAF; In tetrahydrofuran; water; initial compound treated with TBAF in THF and water; elem. anal.;
DOI:10.1246/cl.2001.554