1-Amino-6,7-dichloroanthraquinone

Base Information

• Chemical Name: 1-Amino-6,7-dichloroanthraquinone
• CAS No.: 5355-88-4
• Molecular Formula: C14H7 Cl2 N O2
• Molecular Weight: 292.121
• Hs Code.: 2922399090
• European Community (EC) Number: 226-340-1
• NSC Number: 239330
• DSSTox Substance ID: DTXSID5063811
• Nikkaji Number: J217.925C
• Wikidata: Q81991025
• Mol file: 5355-88-4.mol

Synonyms:1-amino-6,7-dichloroanthracene-9,10-dione;5355-88-4;1-Amino-6,7-dichloroanthraquinone;Anthraquinone, 1-amino-6,7-dichloro-;EINECS 226-340-1;9,10-Anthracenedione, 1-amino-6,7-dichloro-;NSC 239330;AI3-62984;NSC239330;9, 1-amino-6,7-dichloro-;SCHEMBL8777809;DTXSID5063811;AKOS024261117;NSC-239330;1-amino-6,7-dichloroanthra-9,10-quinone;1-Amino-6,7-dichloro-9,10-anthracenedione;1-AMINO-6,7-DICHLORO-9,10-DIHYDROANTHRACENE-9,10-DIONE

Chemical Property of 1-Amino-6,7-dichloroanthraquinone

Chemical Property:

• Vapor Pressure: 3.75E-05mmHg at 25°C
• Boiling Point: 527.9°Cat760mmHg
• Flash Point: 273.1°C
• PSA: 60.16000
• Density: 1.576g/cm³
• LogP: 3.93220
• XLogP3: 4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 290.9853839
• Heavy Atom Count: 19
• Complexity: 414

Purity/Quality:

1-Amino-6,7-dichloroanthracene-9,10-dione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1=CC2=C(C(=C1)N)C(=O)C3=CC(=C(C=C3C2=O)Cl)Cl

Technology Process of 1-Amino-6,7-dichloroanthraquinone

There total 3 articles about 1-Amino-6,7-dichloroanthraquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6,7-dichloro-1-nitro-anthraquinone (100526-66-7) → 1-amino-6,7-dichloro-anthraquinone (5355-88-4)

Guidance literature:

With sodium hydrogensulfide; water;

Reference yield:

2,3-dichloro-anthraquinone (84-45-7) → 1-amino-6,7-dichloro-anthraquinone (5355-88-4)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂SO₄; HNO₃

2: NaHS; H₂O

With sodium hydrogensulfide; sulfuric acid; water; nitric acid;

Reference yield:

→ 1-amino-6,7-dichloro-anthraquinone (5355-88-4)

Guidance literature:

Dichloranthrachinon (II), 1.)HNO3; 2.)NaSH;

upstream raw materials:

6,7-dichloro-1-nitro-anthraquinone

2,3-dichloro-anthraquinone

Downstream raw materials:

6,7-Dichloro-anthracene-1-carboxylic acid