N,N'-bis(cyclohexyl)methylamidinate gadolinium(III)

Base Information

• Chemical Name: N,N'-bis(cyclohexyl)methylamidinate gadolinium(III)
• CAS No.: 484031-98-3
• Molecular Formula: C₄₂H₇₅GdN₆
• Molecular Weight: 821.348

Synonyms:

Chemical Property of N,N'-bis(cyclohexyl)methylamidinate gadolinium(III)

Chemical Property:

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Technology Process of N,N'-bis(cyclohexyl)methylamidinate gadolinium(III)

There total 1 articles about N,N'-bis(cyclohexyl)methylamidinate gadolinium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N,N'-bis(cyclohexyl)methylamidinate lithium + gadolinium(III) chloride (10138-52-0) → N,N'-bis(cyclohexyl)methylamidinate gadolinium(III) (484031-98-3)

Guidance literature:

In tetrahydrofuran; byproducts: LiCl; under Ar; by a react. of (CyNC(Me)NCy)Li (20.7 mmol) and GdCl3 (6.90 mmol) in THF; stirring for 24 h; the soln. was evapd. to dry in vac.; the residue was extd. with Et2O andLiCl was removed by centrifugation; the exts. were concd. and cooled to -20°C; crystn. from toluene; elem. anal.;

DOI:10.1016/S0022-328X(02)01902-2

upstream raw materials:

gadolinium(III) chloride

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