C₃₃H₄₁N₇O₆P₂

Base Information

Chemical Name:C₃₃H₄₁N₇O₆P₂
CAS No.:1421533-55-2
Molecular Formula:C₃₃H₄₁N₇O₆P₂
Molecular Weight:693.679
Hs Code.:

C<sub>33</sub>H<sub>41</sub>N<sub>7</sub>O<sub>6</sub>P<sub>2</sub>

Synonyms:

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Chemical Property of C₃₃H₄₁N₇O₆P₂

Chemical Property:

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Technology Process of C₃₃H₄₁N₇O₆P₂

There total 4 articles about C₃₃H₄₁N₇O₆P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421533-54-1
diethyl(4-azido-3,5-dimethylphenyl)phosphonate

: 75867-46-8
2,6-diethynylpyridine

: 1421533-55-2
C₃₃H₄₁N₇O₆P₂

Guidance literature:: With tetrakis(actonitrile)copper(I) hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; at 20 ℃; for 48h;
DOI:10.1021/ja310965h

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 1421533-55-2
C₃₃H₄₁N₇O₆P₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: Iodine monochloride / dichloromethane; methanol / 20 °C

2.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 12 h / Reflux; Inert atmosphere

3.1: sodium nitrite / acetic acid; water / 0 °C

3.2: 0 - 20 °C

4.1: N-ethyl-N,N-diisopropylamine; tetrakis(actonitrile)copper(I) hexafluorophosphate / dichloromethane; methanol / 48 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrakis(actonitrile)copper(I) hexafluorophosphate; Iodine monochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium nitrite; In methanol; dichloromethane; water; acetic acid; toluene;
DOI:10.1021/ja310965h

Reference yield:

: 4102-53-8
4-iodo-2,6-dimethylaniline

: 1421533-55-2
C₃₃H₄₁N₇O₆P₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 12 h / Reflux; Inert atmosphere

2.1: sodium nitrite / acetic acid; water / 0 °C

2.2: 0 - 20 °C

3.1: N-ethyl-N,N-diisopropylamine; tetrakis(actonitrile)copper(I) hexafluorophosphate / dichloromethane; methanol / 48 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrakis(actonitrile)copper(I) hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium nitrite; In methanol; dichloromethane; water; acetic acid; toluene;
DOI:10.1021/ja310965h