(3,5-dimethylphenyl)(1-diphenylphosphanyl-1H-pyrrol-2-ylmethylene)amine nickel dibromide

Base Information

Chemical Name:(3,5-dimethylphenyl)(1-diphenylphosphanyl-1H-pyrrol-2-ylmethylene)amine nickel dibromide
CAS No.:918630-23-6
Molecular Formula:C₂₅H₂₃Br₂N₂NiP
Molecular Weight:600.943
Hs Code.:

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Chemical Property of (3,5-dimethylphenyl)(1-diphenylphosphanyl-1H-pyrrol-2-ylmethylene)amine nickel dibromide

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Technology Process of (3,5-dimethylphenyl)(1-diphenylphosphanyl-1H-pyrrol-2-ylmethylene)amine nickel dibromide

There total 2 articles about (3,5-dimethylphenyl)(1-diphenylphosphanyl-1H-pyrrol-2-ylmethylene)amine nickel dibromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 918629-91-1
(3,5-dimethylphenyl)(1-diphenylphosphanyl-1H-pyrrol-2-ylmethylene)amine

: 36673-36-6,111408-20-9,14126-37-5,54053-52-0
dibromobis(triphenylphosphine)nickel(II)

: 918630-23-6
(3,5-dimethylphenyl)(1-diphenylphosphanyl-1H-pyrrol-2-ylmethylene)amine nickel dibromide

Guidance literature:: In acetonitrile; addn. of soln. of N-pyrrolylphosphino-N'-aldimine in CH3CN to a soln. ofNiBr2(PPh3)2 in CH3CN under N2, stirring for 18 h at room temp.; removal of volatiles in vac., extraction with hexane, drying in vac., elem. anal.;
DOI:10.1039/b611652c

Reference yield: 47.0%

: 918629-91-1
(3,5-dimethylphenyl)(1-diphenylphosphanyl-1H-pyrrol-2-ylmethylene)amine

: nickel(II) bromide dimethoxyethane

: 918630-23-6
(3,5-dimethylphenyl)(1-diphenylphosphanyl-1H-pyrrol-2-ylmethylene)amine nickel dibromide

Guidance literature:: In acetonitrile; addn. of soln. of N-pyrrolylphosphino-N'-aldimine in CH3CN to a suspn. of NiBr2(DME) in CH3CN under N2, stirring for 3 h; sepn. of ppt. by filtration, washing with hexane, drying in vac., elem. anal.;
DOI:10.1039/b611652c