1-benzyl-1,2,3-triazole-4,5-dicarboxylic acid diazide

Base Information

• Chemical Name: 1-benzyl-1,2,3-triazole-4,5-dicarboxylic acid diazide
• CAS No.: 1335130-16-9
• Molecular Formula: C₁₁H₇N₉O₂
• Molecular Weight: 297.236
• Mol file: 1335130-16-9.mol

Synonyms:

Chemical Property of 1-benzyl-1,2,3-triazole-4,5-dicarboxylic acid diazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-benzyl-1,2,3-triazole-4,5-dicarboxylic acid diazide

There total 2 articles about 1-benzyl-1,2,3-triazole-4,5-dicarboxylic acid diazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-benzyl-1,2,3-triazole-4,5-dicarboxylic acid dichloride → 1-benzyl-1,2,3-triazole-4,5-dicarboxylic acid diazide (1335130-16-9)

Guidance literature:

With sodium azide; N-benzyl-N,N,N-triethylammonium chloride; In diethyl ether; water; at 20 ℃;

DOI:10.1007/s10593-011-0781-5

Reference yield:

1-benzyl-1H-[1,2,3]-triazole-4,5-dicarboxylic acid (73953-89-6) → 1-benzyl-1,2,3-triazole-4,5-dicarboxylic acid diazide (1335130-16-9)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus pentachloride / benzene / 2 h / 20 °C

2: sodium azide; N-benzyl-N,N,N-triethylammonium chloride / diethyl ether; water / 20 °C

With sodium azide; phosphorus pentachloride; N-benzyl-N,N,N-triethylammonium chloride; In diethyl ether; water; benzene;

DOI:10.1007/s10593-011-0781-5

upstream raw materials:

1-benzyl-1H-[1,2,3]-triazole-4,5-dicarboxylic acid