Phosphine, [bis(2,4,6-trimethylphenyl)germylene][2,4,6-tris(1-methylethyl)phenyl]-

Base Information

Chemical Name:Phosphine, [bis(2,4,6-trimethylphenyl)germylene][2,4,6-tris(1-methylethyl)phenyl]-
CAS No.:137932-03-7
Molecular Formula:C₃₃H₄₅GeP
Molecular Weight:545.284
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphine, [bis(2,4,6-trimethylphenyl)germylene][2,4,6-tris(1-methylethyl)phenyl]-

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Technology Process of Phosphine, [bis(2,4,6-trimethylphenyl)germylene][2,4,6-tris(1-methylethyl)phenyl]-

There total 2 articles about Phosphine, [bis(2,4,6-trimethylphenyl)germylene][2,4,6-tris(1-methylethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 96481-36-6
dimesityldifluorogermane

: 2,4,6-tri-i-propylphenyldilithiophosphide

: 137932-03-7
Mes₂GePIs

Guidance literature:: In not given; byproducts: LiF;

Reference yield: 85.0%

: 109-72-8,29786-93-4
n-butyllithium

: 96481-36-6
dimesityldifluorogermane

: 112438-22-9
(2,4,6-triisopropylphenyl)phosphine

: 137932-03-7
Mes₂GePIs

Guidance literature:: In diethyl ether; byproducts: LiF; on addition of two equivalents of n-butyllithium (1.6M in hexane) to soln. of isitylphosphine in Et2O, followed by 1h stirring at room temp.; the yellow-orange soln. of IsPLi2 was then added to a suspension of ((CH3)3C6H2)2F2Ge in Et2O at -78°C;; the mixture was allowed to warm up at room temp., after 1h stirring at 20°C, the 31PNMR spectrum of the crude solution indicated the nearly quantitative formation of the expected germaphosphene; not isolated;;
DOI:10.1016/0022-328X(91)80132-4