α-methyl-β,β-dichlorovinyl phenyl sulfone

Base Information

• Chemical Name: α-methyl-β,β-dichlorovinyl phenyl sulfone
• CAS No.: 3559-70-4
• Molecular Formula: C₉H₈Cl₂O₂S
• Molecular Weight: 251.133
• Mol file: 3559-70-4.mol

Synonyms:

Chemical Property of α-methyl-β,β-dichlorovinyl phenyl sulfone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-methyl-β,β-dichlorovinyl phenyl sulfone

There total 3 articles about α-methyl-β,β-dichlorovinyl phenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

α-methyl-β,β-dichlorovinyl phenyl sulfide (3559-68-0) → α-methyl-β,β-dichlorovinyl phenyl sulfone (3559-70-4)

Guidance literature:

With dihydrogen peroxide; In acetic acid;

DOI:10.1021/jo01020a076

Reference yield:

Ethyl phenyl sulfide (622-38-8) → α-methyl-β,β-dichlorovinyl phenyl sulfone (3559-70-4)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) NaOMe, petroleum ether, (ii) KOtBu

2: aq. H₂O₂ / acetic acid

With dihydrogen peroxide; In acetic acid;

DOI:10.1021/jo01020a076

Reference yield:

thiophenol (108-98-5) → α-methyl-β,β-dichlorovinyl phenyl sulfone (3559-70-4)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl

2: aq. H₂O₂ / acetic acid

With hydrogenchloride; dihydrogen peroxide; In acetic acid;

DOI:10.1021/jo01020a076

upstream raw materials:

α-methyl-β,β-dichlorovinyl phenyl sulfide

Ethyl phenyl sulfide

thiophenol