Technology Process of C28H34N4O4S
There total 7 articles about C28H34N4O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran
2: toluene-4-sulfonic acid / 1,4-dioxane / 60 °C
3: trifluoroacetic acid / dichloromethane
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide
5: manganese(IV) oxide / dichloromethane
6: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane
With
manganese(IV) oxide; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.11.112
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene-4-sulfonic acid / 1,4-dioxane / 60 °C
2: trifluoroacetic acid / dichloromethane
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide
4: manganese(IV) oxide / dichloromethane
5: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane
With
manganese(IV) oxide; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
1,4-dioxane; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.11.112
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trifluoroacetic acid / dichloromethane
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide
3: manganese(IV) oxide / dichloromethane
4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane
With
manganese(IV) oxide; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.11.112