2,3-Dichlor-1,3-diphenyl-propenon

Base Information

• Chemical Name: 2,3-Dichlor-1,3-diphenyl-propenon
• CAS No.: 13524-02-2
• Molecular Formula: C₁₅H₁₀Cl₂O
• Molecular Weight: 277.15
• Mol file: 13524-02-2.mol

Synonyms:

Chemical Property of 2,3-Dichlor-1,3-diphenyl-propenon

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-Dichlor-1,3-diphenyl-propenon

There total 1 articles about 2,3-Dichlor-1,3-diphenyl-propenon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

1,3-diphenyl-2-propynone (7338-94-5) → 2,3-Dichlor-1,3-diphenyl-propenon (13524-02-2,13524-12-4)

Guidance literature:

With acrylic acid n-butyl ester; copper dichloride; palladium dichloride; In acetonitrile; for 12h;

DOI:10.1021/acs.orglett.9b03066

Reference yield:

2,3-Dichlor-1,3-diphenyl-propenon (13524-02-2,13524-12-4) → 1,3-Diphenyl-1,2,3,3-tetrachlor-propen (13524-13-5)

Guidance literature:

With phosphorus pentachloride; In dichloromethane; Heating;

DOI:10.1021/jo01349a517

Reference yield:

2,3-Dichlor-1,3-diphenyl-propenon (13524-02-2,13524-12-4) → 1,2-Dichlor-3,3-dimethoxy-1,3-diphenyl-prop-2-en (13492-69-8)

Guidance literature:

Multi-step reaction with 2 steps

1: PCl₅ / CH₂Cl₂ / Heating

With phosphorus pentachloride; In dichloromethane;

DOI:10.1021/jo01349a517

upstream raw materials:

1,3-diphenyl-2-propynone

Downstream raw materials:

1,3-Diphenyl-1,2,3,3-tetrachlor-propen

1,2-Dichlor-3,3-dimethoxy-1,3-diphenyl-prop-2-en