Technology Process of C26H30N4O4
There total 1 articles about C26H30N4O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 0 - 20 ℃;
DOI:10.1021/jm300664y
- Guidance literature:
-
With
hydrogenchloride;
In
ethyl acetate;
at 20 ℃;
for 2h;
DOI:10.1021/jm300664y
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride / ethyl acetate / 2 h / 20 °C
2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C
2.2: 0 - 20 °C
3.1: hydrogenchloride / ethyl acetate / 2 h / 20 °C
With
hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; ethyl acetate;
DOI:10.1021/jm300664y