BF₄^(1-)*C₃₁H₃₁N₂⁽¹⁺⁾

Base Information

Chemical Name:BF₄^(1-)*C₃₁H₃₁N₂⁽¹⁺⁾
CAS No.:1332883-49-4
Molecular Formula:BF₄*C₃₁H₃₁N₂
Molecular Weight:518.405
Hs Code.:

BF<sub>4</sub><sup>(1-)</sup>*C<sub>31</sub>H<sub>31</sub>N<sub>2</sub><sup>(1+)</sup>

Synonyms:

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Chemical Property of BF₄^(1-)*C₃₁H₃₁N₂⁽¹⁺⁾

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Technology Process of BF₄^(1-)*C₃₁H₃₁N₂⁽¹⁺⁾

There total 3 articles about BF₄^(1-)*C₃₁H₃₁N₂⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 689260-53-5
2-bromo-5-iodo-1,3-dimethylbenzene

: 1332883-49-4
BF₄^(1-)*C₃₁H₃₁N₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; sodium carbonate; triphenylphosphine; phenylboronic acid / water; acetone / 18 h / Reflux; Inert atmosphere

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 44 h / 100 °C / Inert atmosphere

3: ammonium tetrafluoroborate; formic acid / 6 h / 120 °C / Inert atmosphere; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; formic acid; ammonium tetrafluoroborate; palladium diacetate; sodium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triphenylphosphine; sodium t-butanolate; phenylboronic acid; In water; acetone; toluene;
DOI:10.1039/c1cc13304g

Reference yield:

: 59557-90-3
4-bromo-3,5-dimethylaniline

: 1332883-49-4
BF₄^(1-)*C₃₁H₃₁N₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid; sodium nitrite / water / 0.42 h / -10 °C / Inert atmosphere

1.2: 2.33 h / -10 - 0 °C / Inert atmosphere

2.1: palladium diacetate; sodium carbonate; triphenylphosphine; phenylboronic acid / water; acetone / 18 h / Reflux; Inert atmosphere

3.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 44 h / 100 °C / Inert atmosphere

4.1: ammonium tetrafluoroborate; formic acid / 6 h / 120 °C / Inert atmosphere; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; formic acid; ammonium tetrafluoroborate; sulfuric acid; palladium diacetate; sodium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triphenylphosphine; sodium t-butanolate; sodium nitrite; phenylboronic acid; In water; acetone; toluene;
DOI:10.1039/c1cc13304g

Reference yield:

: 756873-19-5
4-bromo-(3,5-dimethyl)biphenyl

: 1332883-49-4
BF₄^(1-)*C₃₁H₃₁N₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 44 h / 100 °C / Inert atmosphere

2: ammonium tetrafluoroborate; formic acid / 6 h / 120 °C / Inert atmosphere; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; formic acid; ammonium tetrafluoroborate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; In toluene;
DOI:10.1039/c1cc13304g