3-[Anilino(phenyl)methyl]-4-hydroxyoxolan-2-one

Base Information

Chemical Name:3-[Anilino(phenyl)methyl]-4-hydroxyoxolan-2-one
CAS No.:137955-75-0
Molecular Formula:C17H17NO3
Molecular Weight:283.327
Hs Code.:
DSSTox Substance ID:DTXSID20566794
Mol file:137955-75-0.mol

Synonyms:137955-75-0;3-[Anilino(phenyl)methyl]-4-hydroxyoxolan-2-one;DTXSID20566794

Suppliers and Price of 3-[Anilino(phenyl)methyl]-4-hydroxyoxolan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-[Anilino(phenyl)methyl]-4-hydroxyoxolan-2-one

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:283.12084340
Heavy Atom Count:21
Complexity:348

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(C(C(=O)O1)C(C2=CC=CC=C2)NC3=CC=CC=C3)O

Technology Process of 3-[Anilino(phenyl)methyl]-4-hydroxyoxolan-2-one

There total 1 articles about 3-[Anilino(phenyl)methyl]-4-hydroxyoxolan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 79687-69-7
3,4-diphenyl-6-oxo-2,7-dioxa-3-azabicyclo<3.3.0>octane

: 137955-75-0
3-hydroxy-2-phenylanilinomethylbutanolide

Guidance literature:: With hydrogen; nickel; In ethyl acetate; at 50 ℃; for 6h; under 760 Torr;

Reference yield: 85.0%

: 108-24-7
acetic anhydride

: 137955-75-0
3-hydroxy-2-phenylanilinomethylbutanolide

: 2-methylperhydro-5,6-furanonyl-1,3-oxazinium perchlorate

Guidance literature:: With perchloric acid; at 0 ℃; for 1h;

Reference yield:

: 137955-75-0
3-hydroxy-2-phenylanilinomethylbutanolide

: 3-acetamido-2-phenylanilinomethylbutanolide

Guidance literature:: Multi-step reaction with 3 steps

1: 33 percent / 70percent HClO₄ / Heating

2: 91 percent / 70percent HClO₄ / acetic anhydride / 0 °C

3: 62 percent / NH₃ (gas) / 0.5 h

With perchloric acid; ammonia; In acetic anhydride;