Technology Process of C26H30O10
There total 14 articles about C26H30O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / H2 / Pd/C / methanol / 4 h
2: 86 percent / Ag2O / 3 h / Heating
3: 45 percent / PCC / CH2Cl2 / 48 h / 4 A mol. sieves
4: 79 percent / NaOMe / methanol / 16 h / 0 - 20 °C
5: pyridinium toluene-p-sulfonate (PPTS) / benzene / 2 h / Heating
With
hydrogen; sodium methylate; pyridinium p-toluenesulfonate; pyridinium chlorochromate; silver(l) oxide;
palladium on activated charcoal;
In
methanol; dichloromethane; benzene;
DOI:10.1039/c39920001304
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 82 percent / H2 / 10percent Pd/C / methanol / 0.33 h
2: 72 percent / pyridinium chlorochromate, molecular sieves 4 Angstroem / CH2Cl2 / 48 h / Ambient temperature
3: 1) NaOMe, 2) PPTS / 1) methanol, 24 h, 2) benzene, reflux, 1 h
With
4 A molecular sieve; hydrogen; sodium methylate; pyridinium p-toluenesulfonate; pyridinium chlorochromate;
palladium on activated charcoal;
In
methanol; dichloromethane;
DOI:10.1016/0040-4039(91)80784-4
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / H2 / Pd/C / methanol / 4 h
2: 86 percent / Ag2O / 3 h / Heating
3: 45 percent / PCC / CH2Cl2 / 48 h / 4 A mol. sieves
4: 79 percent / NaOMe / methanol / 16 h / 0 - 20 °C
5: pyridinium toluene-p-sulfonate (PPTS) / benzene / 2 h / Heating
With
hydrogen; sodium methylate; pyridinium p-toluenesulfonate; pyridinium chlorochromate; silver(l) oxide;
palladium on activated charcoal;
In
methanol; dichloromethane; benzene;
DOI:10.1039/c39920001304
