N--3,5-dimethyl-4-methoxy-phenylalanin-benzylester

Base Information

• Chemical Name: N--3,5-dimethyl-4-methoxy-phenylalanin-benzylester
• CAS No.: 22741-32-8
• Molecular Formula: C₃₀H₃₄N₂O₅
• Molecular Weight: 502.61
• Mol file: 22741-32-8.mol

Synonyms:

Chemical Property of N--3,5-dimethyl-4-methoxy-phenylalanin-benzylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N--3,5-dimethyl-4-methoxy-phenylalanin-benzylester

There total 4 articles about N--3,5-dimethyl-4-methoxy-phenylalanin-benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-benzyl-5-methyl-imidazolidine-2,4-dione (27993-44-8) → N--3,5-dimethyl-4-methoxy-phenylalanin-benzylester (22741-32-8)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. NaOH / Heating

2: Ac₂O

3: (i) Et₃N, (ii) /BRN= 2724475/, DCC

With sodium hydroxide; acetic anhydride;

Reference yield:

2-methyl-3-phenylalanine (1132-26-9) → N--3,5-dimethyl-4-methoxy-phenylalanin-benzylester (22741-32-8)

Guidance literature:

Multi-step reaction with 2 steps

1: Ac₂O

2: (i) Et₃N, (ii) /BRN= 2724475/, DCC

With acetic anhydride;

Reference yield:

2-Benzyl-2-(formylamino)-propionsaeure (23082-21-5) + 2-Amino-3-(4-methoxy-3,5-dimethyl-phenyl)-propionic acid benzyl ester; hydrochloride → N--3,5-dimethyl-4-methoxy-phenylalanin-benzylester (22741-32-8)

Guidance literature:

Multistep reaction; (i) Et₃N, (ii) /BRN= 2724475/, DCC;

upstream raw materials:

2-Benzyl-2-(formylamino)-propionsaeure

5-benzyl-5-methyl-imidazolidine-2,4-dione

2-methyl-3-phenylalanine

Downstream raw materials:

2-(2-Formylamino-2-methyl-3-phenyl-propionylamino)-3-(4-methoxy-3,5-dimethyl-phenyl)-propionic acid

N-<α-Methyl-phenyl-alanyl>-3,5-dimethyl-4-methoxy-phenylalanin