C₁₉H₂₂N₂O₂S

Base Information

Chemical Name:C₁₉H₂₂N₂O₂S
CAS No.:1349067-26-0
Molecular Formula:C₁₉H₂₂N₂O₂S
Molecular Weight:342.462
Hs Code.:

C<sub>19</sub>H<sub>22</sub>N<sub>2</sub>O<sub>2</sub>S

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Chemical Property of C₁₉H₂₂N₂O₂S

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Technology Process of C₁₉H₂₂N₂O₂S

There total 7 articles about C₁₉H₂₂N₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1349067-24-8
C₁₃H₁₆N₂O₂

: 108-98-5
thiophenol

: 1349067-26-0
C₁₉H₂₂N₂O₂S

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In toluene; tert-butyl alcohol; for 22h; Reflux; Inert atmosphere;
DOI:10.1021/ol202769f

Reference yield:

: 1003049-46-4
C₁₀H₁₀Cl₃NO₂

: 1349067-26-0
C₁₉H₂₂N₂O₂S

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetyl chloride / 20 h / Reflux; Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 72 h / 20 °C / Inert atmosphere

3.1: water; sodium hydroxide / methanol / 3 h / 50 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine; HATU / acetonitrile / 20 °C / Inert atmosphere

5.1: water; trifluoroacetic acid / dichloromethane / 4 h / Inert atmosphere

5.2: 3 h / 0 °C / Inert atmosphere

5.3: 20 h / 0 - 20 °C / Inert atmosphere

6.1: 2,2'-azobis(isobutyronitrile) / toluene; tert-butyl alcohol / 22 h / Reflux; Inert atmosphere

With 2,2'-azobis(isobutyronitrile); water; N-ethyl-N,N-diisopropylamine; acetyl chloride; HATU; trifluoroacetic acid; sodium hydroxide; In methanol; dichloromethane; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ol202769f

Reference yield:

: 1349067-59-9
C₁₄H₂₁NO₄

: 1349067-26-0
C₁₉H₂₂N₂O₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; sodium hydroxide / methanol / 3 h / 50 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine; HATU / acetonitrile / 20 °C / Inert atmosphere

3.1: water; trifluoroacetic acid / dichloromethane / 4 h / Inert atmosphere

3.2: 3 h / 0 °C / Inert atmosphere

3.3: 20 h / 0 - 20 °C / Inert atmosphere

4.1: 2,2'-azobis(isobutyronitrile) / toluene; tert-butyl alcohol / 22 h / Reflux; Inert atmosphere

With 2,2'-azobis(isobutyronitrile); water; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; sodium hydroxide; In methanol; dichloromethane; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ol202769f