(P(C₆H₁₁)3)2NiCl

Base Information

• Chemical Name: (P(C₆H₁₁)3)2NiCl
• CAS No.: 84291-94-1
• Molecular Formula: C₃₆H₆₆ClNiP₂
• Molecular Weight: 655.011
• Mol file: 84291-94-1.mol

Synonyms:

Chemical Property of (P(C₆H₁₁)3)2NiCl

Chemical Property:

Purity/Quality:

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Technology Process of (P(C₆H₁₁)3)2NiCl

There total 1 articles about (P(C₆H₁₁)3)2NiCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

bis(1,5-cyclooctadiene)nickel(0) (1295-35-8) + (1,2-dimethoxyethane)dichloronickel(II) (29046-78-4) + tricyclohexylphosphine (2622-14-2) → (P(C6H11)3)2NiCl (84291-94-1)

Guidance literature:

In toluene; at 20 ℃; for 22h; Schlenk technique; Inert atmosphere;

DOI:10.1021/jacs.6b11412

Reference yield:

(P(C6H11)3)2NiCl (84291-94-1) + tricyclohexylphosphine (2622-14-2) → NiCl(P(C6H11)3)3

Guidance literature:

In toluene; no react. in presence of a significant excess of phosphine;;

upstream raw materials:

bis(1,5-cyclooctadiene)nickel⁽⁰⁾

(1,2-dimethoxyethane)dichloronickel(II)

tricyclohexylphosphine