3-Oxazolidinecarboxylic acid, 4-[(5-methoxy-4-phenoxy-1,4-cyclohexadien-1-yl)carbonyl]-2,2-dimethyl- , phenylmethyl ester, (R)-

Base Information

Chemical Name:3-Oxazolidinecarboxylic acid, 4-[(5-methoxy-4-phenoxy-1,4-cyclohexadien-1-yl)carbonyl]-2,2-dimethyl- , phenylmethyl ester, (R)-
CAS No.:137960-04-4
Molecular Formula:C₂₇H₂₉NO₆
Molecular Weight:463.53
Hs Code.:
Mol file:137960-04-4.mol

Synonyms:

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Chemical Property of 3-Oxazolidinecarboxylic acid, 4-[(5-methoxy-4-phenoxy-1,4-cyclohexadien-1-yl)carbonyl]-2,2-dimethyl- , phenylmethyl ester, (R)-

Chemical Property:

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Technology Process of 3-Oxazolidinecarboxylic acid, 4-[(5-methoxy-4-phenoxy-1,4-cyclohexadien-1-yl)carbonyl]-2,2-dimethyl- , phenylmethyl ester, (R)-

There total 3 articles about 3-Oxazolidinecarboxylic acid, 4-[(5-methoxy-4-phenoxy-1,4-cyclohexadien-1-yl)carbonyl]-2,2-dimethyl- , phenylmethyl ester, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133464-37-6
(4R)-4-formyl-2,2-dimethyloxazolidine-3-carboxylic acid benzyl ester

: 137960-04-4
(R)-4-(5-Methoxy-4-phenoxy-cyclohexa-1,4-dienecarbonyl)-2,2-dimethyl-oxazolidine-3-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

2: Jones' reagent

3: toluene / 60 h / 150 °C

With jones' reagent; In toluene;
DOI:10.1016/S0040-4039(00)93539-1

Reference yield:

: Benzyl (R)-4-(1-hydroxy-2-propynyl)-2,2-dimethyl-3-oxazolidinecarboxylate

: 137960-04-4
(R)-4-(5-Methoxy-4-phenoxy-cyclohexa-1,4-dienecarbonyl)-2,2-dimethyl-oxazolidine-3-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Jones' reagent

2: toluene / 60 h / 150 °C

With jones' reagent; In toluene;
DOI:10.1016/S0040-4039(00)93539-1

Reference yield:

: 137960-01-1
2-Methoxy-3-phenoxy-1,3-butadiene

: 137960-00-0
Benzyl (R)-4-(1-oxo-2-propynyl)-2,2-dimethyl-3-oxazolidinecarboxylate

: 137960-04-4
(R)-4-(5-Methoxy-4-phenoxy-cyclohexa-1,4-dienecarbonyl)-2,2-dimethyl-oxazolidine-3-carboxylic acid benzyl ester

: 137960-03-3
(R)-4-(4-Methoxy-5-phenoxy-cyclohexa-1,4-dienecarbonyl)-2,2-dimethyl-oxazolidine-3-carboxylic acid benzyl ester

Guidance literature:: In toluene; at 150 ℃; for 60h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(00)93539-1