C₂₈H₃₀O₅

Base Information

• Chemical Name: C₂₈H₃₀O₅
• CAS No.: 1373318-92-3
• Molecular Formula: C₂₈H₃₀O₅
• Molecular Weight: 446.543

Synonyms:

Chemical Property of C₂₈H₃₀O₅

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₂₈H₃₀O₅

There total 2 articles about C₂₈H₃₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

C35H42O6 (1373318-90-1) → cyclohexylmethyl 2,4-di-O-benzyl-3,6-O-(o-xylylene)-β-D-glucopyranoside (1181209-03-9) + C28H30O5 (1373318-92-3)

Guidance literature:

With hydrogen tetrakis(pentafluorophenyl)borate; t-butyl bromide; silver tetrakis(pentafluorophenyl)borate; In α,α,α-trifluorotoluene; at 20 ℃; for 0.916667h; Inert atmosphere; Molecular sieve;

DOI:10.1021/ja301480g

Reference yield:

2,4-di-O-benzyl-3,6-O-(o-xylylene)-D-glucopyranosyl fluoride → C28H30O5 (1373318-92-3)

Guidance literature:

Multi-step reaction with 2 steps

1: stannous fluoride; t-butyl bromide; silver tetrakis(pentafluorophenyl)borate / α,α,α-trifluorotoluene / 16 h / 20 °C / Inert atmosphere; Molecular sieve

2: hydrogen tetrakis(pentafluorophenyl)borate; t-butyl bromide; silver tetrakis(pentafluorophenyl)borate / α,α,α-trifluorotoluene / 0.92 h / 20 °C / Inert atmosphere; Molecular sieve

With hydrogen tetrakis(pentafluorophenyl)borate; stannous fluoride; t-butyl bromide; silver tetrakis(pentafluorophenyl)borate; In α,α,α-trifluorotoluene;

DOI:10.1021/ja301480g

upstream raw materials:

C₃₅H₄₂O₆

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