allyl O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1<>4)-O-(2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1<>4)-2-acetamido-3,6-di-O-(2-butenyl)-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:allyl O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1<*>4)-O-(2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1<*>4)-2-acetamido-3,6-di-O-(2-butenyl)-2-deoxy-β-D-glucopyranoside
CAS No.:74653-23-9
Molecular Formula:C₆₈H₈₄N₂O₁₆
Molecular Weight:1185.42
Hs Code.:

allyl O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1<*>4)-O-(2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1<*>4)-2-acetamido-3,6-di-O-(2-butenyl)-2-deoxy-β-D-glucopyranoside

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Chemical Property of allyl O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1<*>4)-O-(2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1<*>4)-2-acetamido-3,6-di-O-(2-butenyl)-2-deoxy-β-D-glucopyranoside

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Technology Process of allyl O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1<*>4)-O-(2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1<*>4)-2-acetamido-3,6-di-O-(2-butenyl)-2-deoxy-β-D-glucopyranoside

There total 9 articles about allyl O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1<*>4)-O-(2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1<*>4)-2-acetamido-3,6-di-O-(2-butenyl)-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: allyl O-(2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1<*>4)-O-(2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1<*>4)-2-acetamido-3,6-di-O-(2-butenyl)-2-deoxy-β-D-glucopyranoside

: 74653-23-9,74653-25-1
allyl O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1<*>4)-O-(2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1<*>4)-2-acetamido-3,6-di-O-(2-butenyl)-2-deoxy-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/S0008-6215(00)85522-6

Reference yield:

: 55659-53-5,77790-47-7,93381-69-2,53270-13-6
2-O-acetyl-3,4,6-tri-O-benzyl-α-D-glucopyranosyl bromide

: 74653-23-9,74653-25-1
allyl O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1<*>4)-O-(2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1<*>4)-2-acetamido-3,6-di-O-(2-butenyl)-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / silver triflate, 1,1,3,3-tetramethylurea / CH₂Cl₂ / 6 h / Ambient temperature

2: 98 percent / sodium methoxide (M) / methanol; CH₂Cl₂ / 24 h / Ambient temperature

With sodium methylate; silver trifluoromethanesulfonate; tetramethylurea; In methanol; dichloromethane;
DOI:10.1016/S0008-6215(00)85522-6

Reference yield:

: 74653-19-3
allyl 2-acetamido-3,6-di-O-(2-butenyl)-2-deoxy-β-D-glucopyranoside

: 74653-23-9,74653-25-1
allyl O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-(1<*>4)-O-(2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1<*>4)-2-acetamido-3,6-di-O-(2-butenyl)-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 30.3 percent / p-toluenesulfonic acid / 1,2-dichloro-ethane / 6 h / Heating

2: sodium methoxide (M) / methanol / 1 h / Ambient temperature

3: 44 percent / silver triflate, 1,1,3,3-tetramethylurea / CH₂Cl₂ / 6 h / Ambient temperature

4: 98 percent / sodium methoxide (M) / methanol; CH₂Cl₂ / 24 h / Ambient temperature

With sodium methylate; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; tetramethylurea; In methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/S0008-6215(00)85522-6