5,9-diphenyl-2,12-dithia-5,9-diphosphatridecane

Base Information

Chemical Name:5,9-diphenyl-2,12-dithia-5,9-diphosphatridecane
CAS No.:187106-42-9
Molecular Formula:C₂₁H₃₀P₂S₂
Molecular Weight:408.549
Hs Code.:

Synonyms:

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Chemical Property of 5,9-diphenyl-2,12-dithia-5,9-diphosphatridecane

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Technology Process of 5,9-diphenyl-2,12-dithia-5,9-diphosphatridecane

There total 1 articles about 5,9-diphenyl-2,12-dithia-5,9-diphosphatridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 542-81-4
sulfure de methyle et de 2-chloroethyle

: 28240-66-6
1,3-bis(phenylphosphano)propane

: 187106-42-9
5,9-diphenyl-2,12-dithia-5,9-diphosphatridecane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; Yield given; 1.) 50 deg C, 1 h; 2.) room temp., overnight;

Reference yield: 36.0%

: lithium tetrafluoroborate

: trans-dichlorotetra(pyridine)cobalt(III) chloride hexahydrate

: 187106-42-9
5,9-diphenyl-2,12-dithia-5,9-diphosphatridecane

: 187106-37-2,187175-26-4
CoCl₂(C₂₁H₃₀P₂S₂)⁽¹⁺⁾*BF₄^(1-) = [CoCl₂(C₂₁H₃₀P₂S₂)]BF₄

: CoCl₂(C₂₁H₃₀P₂S₂)⁽¹⁺⁾*BF₄^(1-) = [CoCl₂(C₂₁H₃₀P₂S₂)]BF₄

Guidance literature:: In methanol; (N2); stirring the Co complex and the ligand in MeOH (room temp., overnight), chromy., addn. of LiBF4 to each of the eluates in MeOH; filtration, recrystn. (MeCN/Et2O); elem. anal.;

Reference yield: 26.8%

: copper(II) tetrafluoroborate tetrahydrate

: 187106-42-9
5,9-diphenyl-2,12-dithia-5,9-diphosphatridecane

: [Cu₂(5,9-diphenyl-5,9-diphospha-2,12-dithiatridecane)2](BF₄)2

Guidance literature:: In methanol; mixing copper salt and ligand in methanol; washing with water, ether, drying in vac.; elem. anal.;
DOI:10.1016/j.ica.2003.08.008