(R)-ethylmethylphenylsilane

Base Information

Chemical Name:(R)-ethylmethylphenylsilane
CAS No.:15943-02-9
Molecular Formula:C₉H₁₄Si
Molecular Weight:150.296
Hs Code.:

Synonyms:

Suppliers and Price of (R)-ethylmethylphenylsilane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (R)-ethylmethylphenylsilane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (R)-ethylmethylphenylsilane

There total 6 articles about (R)-ethylmethylphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 149-74-6
dichloromethylphenylsilane

: 15943-02-9
(R)-ethylmethylphenylsilane

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / pyridine / benzene / 3 h / 70 - 80 °C

2: diethyl ether / 0.5 h / -70 °C

3: diethyl ether

4: LiAlH₄

With pyridine; lithium aluminium tetrahydride; In diethyl ether; benzene; 1: Condensation / 2: Ring cleavage / 3: silylation / 4: Reduction;
DOI:10.1246/bcsj.70.1393

Reference yield:

: 925-90-6
ethylmagnesium bromide

: 111949-28-1
(5S,6S)-5,6-dimethoxy-2-methyl-2-phenyl-1,3-dioxa-2-silacycloheptane

: 15943-02-9
(R)-ethylmethylphenylsilane

: 15726-87-1
(S)-ethylmethylphenylsilane

Guidance literature:: ethylmagnesium bromide; (5S,6S)-5,6-dimethoxy-2-methyl-2-phenyl-1,3-dioxa-2-silacycloheptane; In diethyl ether; at -70 ℃; for 0.5h;

With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 1h; Title compound not separated from byproducts;
DOI:10.1246/bcsj.70.1393

Reference yield:

: 111949-28-1
(5S,6S)-5,6-dimethoxy-2-methyl-2-phenyl-1,3-dioxa-2-silacycloheptane

: 15943-02-9
(R)-ethylmethylphenylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 0.5 h / -70 °C

2: diethyl ether

3: LiAlH₄

With lithium aluminium tetrahydride; In diethyl ether; 1: Ring cleavage / 2: silylation / 3: Reduction;
DOI:10.1246/bcsj.70.1393