4-[5-(3-Hydroxymethylbenzyloxycarbonyl)-3-(2-methoxycarbonylethyl)-4-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8-bis(2-methoxycarbonylethyl)-3,7-bis(methoxycarbonylmethyl)-9-(2-trimethylsilylethoxycarbonyl)-4,5-dihydrodipyrrin-1(10H)-one

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Chemical Name:4-[5-(3-Hydroxymethylbenzyloxycarbonyl)-3-(2-methoxycarbonylethyl)-4-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8-bis(2-methoxycarbonylethyl)-3,7-bis(methoxycarbonylmethyl)-9-(2-trimethylsilylethoxycarbonyl)-4,5-dihydrodipyrrin-1(10H)-one
CAS No.:207981-96-2
Molecular Formula:C₅₀H₆₅N₃O₁₈Si
Molecular Weight:1024.16
Hs Code.:

4-[5-(3-Hydroxymethylbenzyloxycarbonyl)-3-(2-methoxycarbonylethyl)-4-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8-bis(2-methoxycarbonylethyl)-3,7-bis(methoxycarbonylmethyl)-9-(2-trimethylsilylethoxycarbonyl)-4,5-dihydrodipyrrin-1(10H)-one

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Chemical Property of 4-[5-(3-Hydroxymethylbenzyloxycarbonyl)-3-(2-methoxycarbonylethyl)-4-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8-bis(2-methoxycarbonylethyl)-3,7-bis(methoxycarbonylmethyl)-9-(2-trimethylsilylethoxycarbonyl)-4,5-dihydrodipyrrin-1(10H)-one

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Technology Process of 4-[5-(3-Hydroxymethylbenzyloxycarbonyl)-3-(2-methoxycarbonylethyl)-4-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8-bis(2-methoxycarbonylethyl)-3,7-bis(methoxycarbonylmethyl)-9-(2-trimethylsilylethoxycarbonyl)-4,5-dihydrodipyrrin-1(10H)-one

There total 2 articles about 4-[5-(3-Hydroxymethylbenzyloxycarbonyl)-3-(2-methoxycarbonylethyl)-4-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8-bis(2-methoxycarbonylethyl)-3,7-bis(methoxycarbonylmethyl)-9-(2-trimethylsilylethoxycarbonyl)-4,5-dihydrodipyrrin-1(10H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 626-18-6
1,3-dimethanol benzene

: C₄₂H₅₇N₃O₁₇Si

: 207981-96-2
4-[5-(3-Hydroxymethylbenzyloxycarbonyl)-3-(2-methoxycarbonylethyl)-4-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8-bis(2-methoxycarbonylethyl)-3,7-bis(methoxycarbonylmethyl)-9-(2-trimethylsilylethoxycarbonyl)-4,5-dihydrodipyrrin-1(10H)-one

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; for 1h; Heating;
DOI:10.1039/a708134k

Reference yield:

: 207981-95-1
4-[5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8-bis(2-methoxycarbonylethyl)-3,7-bis(methoxycarbonylmethyl)-9-(2-trimethylsilylethoxycarbonyl)-4,5-dihydrodipyrrin-1(10H)-one

: 207981-96-2
4-[5-(3-Hydroxymethylbenzyloxycarbonyl)-3-(2-methoxycarbonylethyl)-4-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8-bis(2-methoxycarbonylethyl)-3,7-bis(methoxycarbonylmethyl)-9-(2-trimethylsilylethoxycarbonyl)-4,5-dihydrodipyrrin-1(10H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂CO₃, H₂ / 10percent Pd/C / methanol

2: 71 percent / DCC, DMAP / tetrahydrofuran / 1 h / Heating

With dmap; hydrogen; sodium carbonate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1039/a708134k