C₁₂H₁₄Br₃NO₂*BrH

Base Information

Chemical Name:C₁₂H₁₄Br₃NO₂*BrH
CAS No.:1452587-03-9
Molecular Formula:BrH*C₁₂H₁₄Br₃NO₂
Molecular Weight:524.873
Hs Code.:

C<sub>12</sub>H<sub>14</sub>Br<sub>3</sub>NO<sub>2</sub>*BrH

Synonyms:

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Chemical Property of C₁₂H₁₄Br₃NO₂*BrH

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Technology Process of C₁₂H₁₄Br₃NO₂*BrH

There total 4 articles about C₁₂H₁₄Br₃NO₂*BrH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 1452587-03-9
C₁₂H₁₄Br₃NO₂*BrH

Guidance literature:: Multi-step reaction with 4 steps

1: pyridinium bromochromate / acetic acid / 2 h / 40 °C

2: potassium carbonate / N,N-dimethyl-formamide / 36 h / 20 °C

3: bromine / chloroform / 2 h / 20 °C

4: hydrogen bromide; water / methanol / 48 h

With pyridinium bromochromate; water; hydrogen bromide; bromine; potassium carbonate; In methanol; chloroform; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.07.017

Reference yield:

: 2887-72-1
1-(3,5-dibromo-4-hydroxyphenyl)ethan-1-one

: 1452587-03-9
C₁₂H₁₄Br₃NO₂*BrH

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 36 h / 20 °C

2: bromine / chloroform / 2 h / 20 °C

3: hydrogen bromide; water / methanol / 48 h

With water; hydrogen bromide; bromine; potassium carbonate; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.07.017

Reference yield:

: 1452587-07-3
C₁₂H₁₃Br₃O₂

: 1452587-03-9
C₁₂H₁₄Br₃NO₂*BrH

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / chloroform / 2 h / 20 °C

2: hydrogen bromide; water / methanol / 48 h

With water; hydrogen bromide; bromine; In methanol; chloroform;
DOI:10.1016/j.bmcl.2013.07.017