N-<<4-O-(2'-acetamido-3',4',6'-tri-O-acetyl-2'-deoxy-β-D-glucopyranosyl)-2-O-benzyl-N-benzyloxycarbonyl-6-O-(tert-butyldimethylsilyl)-1,3,5-trideoxy-1,5-imino-D-mannitol-3-yloxy>acetyl>-L-Ala-γ-D-Glu-(N^ε-benzyloxycarbonyl)-L-Lys dibenzyl ester

Base Information

• Chemical Name: N-<<4-O-(2'-acetamido-3',4',6'-tri-O-acetyl-2'-deoxy-β-D-glucopyranosyl)-2-O-benzyl-N-benzyloxycarbonyl-6-O-(tert-butyldimethylsilyl)-1,3,5-trideoxy-1,5-imino-D-mannitol-3-yloxy>acetyl>-L-Ala-γ-D-Glu-(N^ε-benzyloxycarbonyl)-L-Lys dibenzyl ester
• CAS No.: 144382-59-2
• Molecular Formula: C₇₉H₁₀₂N₆O₂₃Si
• Molecular Weight: 1531.79

Synonyms:

Chemical Property of N-<<4-O-(2'-acetamido-3',4',6'-tri-O-acetyl-2'-deoxy-β-D-glucopyranosyl)-2-O-benzyl-N-benzyloxycarbonyl-6-O-(tert-butyldimethylsilyl)-1,3,5-trideoxy-1,5-imino-D-mannitol-3-yloxy>acetyl>-L-Ala-γ-D-Glu-(N^ε-benzyloxycarbonyl)-L-Lys dibenzyl ester

Chemical Property:

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Technology Process of N-<<4-O-(2'-acetamido-3',4',6'-tri-O-acetyl-2'-deoxy-β-D-glucopyranosyl)-2-O-benzyl-N-benzyloxycarbonyl-6-O-(tert-butyldimethylsilyl)-1,3,5-trideoxy-1,5-imino-D-mannitol-3-yloxy>acetyl>-L-Ala-γ-D-Glu-(N^ε-benzyloxycarbonyl)-L-Lys dibenzyl ester

There total 1 articles about N-<<4-O-(2'-acetamido-3',4',6'-tri-O-acetyl-2'-deoxy-β-D-glucopyranosyl)-2-O-benzyl-N-benzyloxycarbonyl-6-O-(tert-butyldimethylsilyl)-1,3,5-trideoxy-1,5-imino-D-mannitol-3-yloxy>acetyl>-L-Ala-γ-D-Glu-(N^ε-benzyloxycarbonyl)-L-Lys dibenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

3-O-(2-acetamido-3',4',6'-tri-O-acetyl-2'-deoxy-β-D-glucopyranosyl)-5-O-benzyl-N-benzyloxycarbonyl-1-O-(tert-butyldimethylsilyl)-4-O-carboxymethyl-D-mannitol (144382-54-7) + L-alanyl-γ-D-glutamyl-ε-(N-benzyloxycarbonyl)-L-lysine dibenzyl ester hydrochloride (144382-62-7) → N-<<4-O-(2'-acetamido-3',4',6'-tri-O-acetyl-2'-deoxy-β-D-glucopyranosyl)-2-O-benzyl-N-benzyloxycarbonyl-6-O-(tert-butyldimethylsilyl)-1,3,5-trideoxy-1,5-imino-D-mannitol-3-yloxy>acetyl>-L-Ala-γ-D-Glu-(Nε-benzyloxycarbonyl)-L-Lys dibenzyl ester (144382-59-2)

Guidance literature:

With 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide; Ambient temperature;

upstream raw materials:

3-O-(2-acetamido-3',4',6'-tri-O-acetyl-2'-deoxy-β-D-glucopyranosyl)-5-O-benzyl-N-benzyloxycarbonyl-1-O-(tert-butyldimethylsilyl)-4-O-carboxymethyl-D-mannitol

L-alanyl-γ-D-glutamyl-ε-(N-benzyloxycarbonyl)-L-lysine dibenzyl ester hydrochloride

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