MnBr(CO)3(P(C₆H₄CH₃)2OSi(CH₃)3)2

Base Information

Chemical Name:MnBr(CO)3(P(C₆H₄CH₃)2OSi(CH₃)3)2
CAS No.:138026-02-5
Molecular Formula:C₃₇H₄₆BrMnO₅P₂Si₂
Molecular Weight:823.73
Hs Code.:

MnBr(CO)3(P(C<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>)2OSi(CH<sub>3</sub>)3)2

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Chemical Property of MnBr(CO)3(P(C₆H₄CH₃)2OSi(CH₃)3)2

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Technology Process of MnBr(CO)3(P(C₆H₄CH₃)2OSi(CH₃)3)2

There total 1 articles about MnBr(CO)3(P(C₆H₄CH₃)2OSi(CH₃)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 14516-54-2
bromopentacarbonylmanganese(I)

: 138150-31-9
(CH₃C₆H₄)2POSi(CH₃)3

: 138026-02-5
MnBr(CO)3(P(C₆H₄CH₃)2OSi(CH₃)3)2

Guidance literature:: In toluene; soln. of (tol)2POSiMe3 in toluene under N2 added to a stirred suspn. of MnBr(CO)5 in toluene at room temp., stirred for 16 h, filtered, concd. to a deep orange soln.,layered with light petroleum ether and cooled to -78°C;; washed with cold (-30°C) petroleum ether,dried in vac.; elem. anal.;;
DOI:10.1016/0022-328X(91)86173-N